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55442-U

Supelco

Supel QuE Verde

Tube, centrifuge tube volume 15 mL, pack of 50 ea

Synonym(s):

Supel QuE, QuEChERS

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About This Item

UNSPSC Code:
41104018
NACRES:
NB.21

material

polypropylene tube

Quality Level

product line

Supel

composition

magnesium sulfate, 1200 mg
Supelclean ENVI-Carb Y, 80 mg
Supelclean PSA, 400 mg
Z-Sep+, 480 mg

packaging

pack of 50 ea

technique(s)

QuEChERS: suitable

centrifuge tube volume

15 mL

matrix active group

PSA phase
carbon phase
zirconia-based phase

application(s)

food and beverages

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General description

Dispersive SPE (dSPE), often referred to as the "QuEChERS" method (Quick, Easy, Cheap, Effective, Rugged, and Safe), is modern sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.

Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.

Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.

Suitability

Designed to provide high recovery all pesticides, including problematic planar pesticides, in samples containing high levels of chlorophyll (e.g. cannabis, spinach, lettuce, oregano, etc.). Ideal for cleanup of extract after initial food extraction and phase partitioning.

Legal Information

AOAC is a registered trademark of AOAC International
ENVI-Carb is a trademark of Sigma-Aldrich Co. LLC
Supel is a trademark of Sigma-Aldrich Co. LLC
Supelclean is a trademark of Sigma-Aldrich Co. LLC

Pictograms

Corrosion

Signal Word

Danger

Hazard Statements

Hazard Classifications

Eye Dam. 1 - Skin Corr. 1B

Storage Class Code

8B - Non-combustible, corrosive hazardous materials

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable


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Articles

Supel™ QuE Verde combines a novel carbon with zirconia coated silica (Z-Sep+) to provide an optimum balance between planar pesticide recovery and color removal.

Compared to conventional PSA/C18/GCB cleanup, cannabis extracts cleaned with the Supel QuE Verde mixture showed lower GC/MS background, and better recoveries for many pesticides.

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