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90479

Supelco

Glyphosate-2-13C,15N

PESTANAL®, analytical standard

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About This Item

Formule linéaire :
HO2C13CH215NHCH2PO3H2
Numéro CAS:
285978-24-7
Poids moléculaire :
171.06
Numéro MDL:
MFCD01075407
Code UNSPSC :
77101502
ID de substance PubChem :
329769915
Nomenclature NACRES :
NA.24

Qualité

analytical standard

Niveau de qualité

200

Gamme de produits

PESTANAL®

Pureté

≥99% (HPLC)

Durée de conservation

limited shelf life, expiry date on the label

Impuretés

≤0.5% water

Pf

230 °C (dec.) (lit.)

Application(s)

agriculture
environmental

Format

neat

Changement de masse

M+2

Chaîne SMILES 

OC(=O)[13CH2][15NH]CP(O)(O)=O

InChI

1S/C3H8NO5P/c5-3(6)1-4-2-10(7,8)9/h4H,1-2H2,(H,5,6)(H2,7,8,9)/i1+1,4+1

Clé InChI

XDDAORKBJWWYJS-VFZPYAPFSA-N

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Description générale

Glyphosate is one of the most used herbicides, especially in agriculture applications such as weed and vegetation control.

Application

Glyphosate-2-13C,15N may be used as a reference standard for the determination of glyphosate-2-13C,15N in saline natural water samples by high-performance liquid chromatography coupled to tandem mass spectrometry (HPLC-MS/MS). It may also be used as an internal standard for the analysis of glyphosate, aminomethylphosphonic acid and glufosinate in water samples by online solid-phase extraction (SPE) followed by HPLC/MS.

Remarque sur l'analyse

13C enrichment ≥99 atom% based upon labeld precursor
15N enrichment ≥98 atom% based upon labeld precursor

Informations légales

PESTANAL is a registered trademark of Merck KGaA, Darmstadt, Germany

Pictogrammes

CorrosionExclamation markEnvironment
GHS05,GHS07,GHS09

Mention d'avertissement

Danger

Mentions de danger

H312,H318,H411

Classification des risques

Acute Tox. 4 Dermal - Aquatic Chronic 2 - Eye Dam. 1

Code de la classe de stockage

11 - Combustible Solids

Classe de danger pour l'eau (WGK)

WGK 2

Point d'éclair (°F)

Not applicable

Point d'éclair (°C)

Not applicable

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Certificats d'analyse (COA)

Lot/Batch Number
BCCJ4513
BCCG3972
BCCB5290
BCBZ3625
BCBW3447

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Consulter la Bibliothèque de documents

Optimization of an Enrichment and LC-MS/MS Method for the Analysis of Glyphosate and Aminomethylphosphonic Acid (AMPA) in Saline Natural Water Samples without Derivatization
Pupke D, et al.
Journal of Chromatography and Separation Techniques, 7(338), 2-2 (2016)
Methods of analysis by the US geological survey organic geochemistry research group-determination of glyphosate, aminomethylphosphonic acid, and glufosinate in water using online solid-phase extraction and high-performance liquid chromatography/mass spectrometry
Lee EA, et al.
Journal of Chromatography and Separation Techniques, 7(338), 2-2 (2002)
Lene Nørby Nielsen et al.
Environmental pollution (Barking, Essex : 1987), 233, 364-376 (2017-11-03)
Recently, concerns have been raised that residues of glyphosate-based herbicides may interfere with the homeostasis of the intestinal bacterial community and thereby affect the health of humans or animals. The biochemical pathway for aromatic amino acid synthesis (Shikimate pathway), which

Articles

LC/MS/MS Method for Determination of Glyphosate, AMPA, and Glufosinate in Cereals

Glyphosate and related compounds are measured in oatmeal and infant cereal using ion-exchange polymer-based particles for HPLC and SPE. Low level detection was obtained.

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