Accéder au contenu
Merck
Toutes les photos(3)

Key Documents

KITALYSISBASE

Sigma-Aldrich

KitAlysis High-Throughput Base Screening Kit - Pack of 2

Synonyme(s) :

Base screen, Base screening kit, KitAlysis base

Se connecterpour consulter vos tarifs contractuels et ceux de votre entreprise/organisme


About This Item

Code UNSPSC :
12161600
Nomenclature NACRES :
NA.22

Capacité de réaction

reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Cross Couplings
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling

Groupe fonctionnel

phosphine

Application

Versatile base screening kit for cross-coupling reactions and other synthetic transformations. Step-by-step user guide and a downloadable experimental excel sheet are provided in the below hyperlinks.

Step-by-Step Guide for KitAlysis High-Throughput Base Reaction Screening Kit

Downloadable experimental excel file

Each kit contains 2 customizable screening sets that contain the following:
  • 7 X 2 pre-weighed bases (30 μmol) in individual microvials with magnetic stir bars
  • 4 X 2 base solutions
  • 2 empty microvials for Chemist′s Choice of base allowing customization
  • 4 degassed anhydrous solvents (DMF, MeOH, THF, Toluene)
  • 2 NEW KitAlysis 24-Well Reaction Block Replacement Films
  • 4 empty substrate stock solution reaction vials with stirbars
Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Caractéristiques et avantages

  • Designed and tested by synthetic chemists
  • Easily run 24-microscale reactions in parallel
  • 10 μmol reactions with 3 equiv. base, 0.1 M concentration
  • Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks

Informations légales

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Composants de kit seuls

Réf. du produit
Description

  • Potassium bicarbonate, ACS reagent, 99.7%, powder, crystals or granules

Composants de kit également disponibles séparément

Réf. du produit
Description
FDS

  • RDD019Potassium phosphate tribasic, anhydrous, free-flowing, Redi-Dri, reagent grade, ≥98%FDS

  • 441902Cesium carbonate, ReagentPlus®, 99%FDS

  • 757551Potassium hydroxide, anhydrous, ≥99.95% trace metals basisFDS

  • 791733Potassium acetate, anhydrous, free-flowing, Redi-Dri, ACS reagent, ≥99.0%FDS

  • 1390091,8-Diazabicyclo[5.4.0]undec-7-ene, 98%FDS

  • 225770Lithium bis(trimethylsilyl)amide solution, 1.0 M in THFFDS

  • 702706Sodium tert-butoxide solution, 2 M in THF, ZerO2®FDS

  • 900522Toluene, anhydrous, ZerO2®, 99.8%FDS

  • 900632Triethylamine, ZerO2®, ≥99%FDS

  • 900636Tetrahydrofuran, anhydrous, inhibitor-free, ZerO2®, ≥99.9%FDS

  • 900638N,N-Dimethylformamide, anhydrous, ZerO2®, 99.8%FDS

  • 900641Methanol, anhydrous, ZerO2®, 99.8%FDS

  • Z118850Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mmFDS

  • Z742110KitAlysis 24-well reaction block replacement filmFDS

  • 900501Potassium carbonate, anhydrous, free-flowing, Redi-Dri, ReagentPlus®, 99%FDS

  • 655104Sodium hydroxide, reagent grade, 97%, powderFDS

Afficher tout (16)

Pictogrammes

FlameHealth hazardCorrosion

Mention d'avertissement

Danger

Mentions de danger

Classification des risques

Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 2 - STOT RE 2 Oral

Organes cibles

Kidney,Adrenal gland,Testes

Risques supp

Code de la classe de stockage

4.1B - Flammable solid hazardous materials

Point d'éclair (°F)

-5.8 °F

Point d'éclair (°C)

-21 °C


Certificats d'analyse (COA)

Recherchez un Certificats d'analyse (COA) en saisissant le numéro de lot du produit. Les numéros de lot figurent sur l'étiquette du produit après les mots "Lot" ou "Batch".

Déjà en possession de ce produit ?

Retrouvez la documentation relative aux produits que vous avez récemment achetés dans la Bibliothèque de documents.

Consulter la Bibliothèque de documents

Articles

KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.

Contenu apparenté

Chemical reaction design and optimization in organic synthesis aims to precisely alter reaction parameters to achieve optimum results in finding pathways to target molecules.

Notre équipe de scientifiques dispose d'une expérience dans tous les secteurs de la recherche, notamment en sciences de la vie, science des matériaux, synthèse chimique, chromatographie, analyse et dans de nombreux autres domaines..

Contacter notre Service technique