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  • The novel and efficient direct synthesis of N,O-acetal compounds using a hypervalent iodine(III) reagent: an improved synthetic method for a key intermediate of discorhabdins.

The novel and efficient direct synthesis of N,O-acetal compounds using a hypervalent iodine(III) reagent: an improved synthetic method for a key intermediate of discorhabdins.

Chemical communications (Cambridge, England) (2005-03-26)
Yu Harayama, Masako Yoshida, Daigo Kamimura, Yasuyuki Kita
RESUMO

The use of hypervalent iodine(III) reagents allowed us to develop the novel and efficient direct synthesis of N,O-acetal compounds via the oxidative fragmentation reaction of alpha-amino acids or alpha-amino alcohols; furthermore, we succeeded in developing an improved synthesis of the key intermediate of discorhabdins.

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Sigma-Aldrich
L-Serine methyl ester hydrochloride, 98%
Sigma-Aldrich
D-Serine methyl ester hydrochloride, 98%
Sigma-Aldrich
DL-Serine methyl ester hydrochloride, 98%