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Key Documents

23307-U

Supelco

SPB®-5

L × I.D. 50 m × 0.32 mm, df 5.00 μm

Synonyme(s) :

GC column, SPB-5, 5% diphenyl

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About This Item

Code UNSPSC :
12000000
eCl@ss :
32119290
Nomenclature NACRES :
SB.54

Matériaux

fused silica

Niveau de qualité

Agence

meets requirements for USP G27 and G36

Paramètres

-60-300 °C temperature (isothermal or programmed)

Valeur bêta

16

df

5.00 μm

Technique(s)

gas chromatography (GC): suitable

L × D.I.

50 m × 0.32 mm

Groupe de la matrice active

Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase

Type de colonne

capillary non-polar

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Description générale

Application: This non-polar general purpose column provides primarily a boiling point elution order with a slight increase in selectivity, especially for aromatic compounds.
USP Code: This column meets USP G27 and G36 requirements.
Phase:
  • Bonded
  • Poly(5% diphenyl/95% dimethyl siloxane)
Temp. Limits:
  • ≤0.32 mm I.D., <2 μm: -60 °C to 320 °C (isothermal or programmed)
  • ≤0.32 mm I.D., ≥2 μm: -60 °C to 300 °C (isothermal or programmed)
  • ≥0.53 mm I.D., <2 μm: -60 °C to 300 °C (isothermal) or 320 °C (programmed)
  • ≥0.53 mm I.D., ≥2 μm: -60 °C to 260 °C (isothermal) or 280 °C (programmed)

Application

SPB®-5 capillary GC column was suitable to investigate high recoveries of polycyclic aromatic hydrocarbons (PAHs) during preparative capillary gas chromatography-mass spectrometry. It may also be used for herbicide determination using In-tube Solid-phase microextraction (SPME).

Autres remarques

We offer a variety of chromatography accessories including analytical syringes

Informations légales

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

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Consulter la Bibliothèque de documents

Manolis Mandalakis et al.
Journal of chromatography. A, 996(1-2), 163-172 (2003-07-02)
Operation parameters of a preparative capillary gas chromatography (pcGC) system were optimized to facilitate clean and efficient harvesting of individual polycyclic aromatic hydrocarbons (PAHs) for subsequent compound-specific radiocarbon analysis. For PAHs, the recommended optimized settings of the specially-designed pcGC cooled
L J Krutz et al.
Journal of chromatography. A, 999(1-2), 103-121 (2003-07-30)
Liquid-liquid extraction or solid-phase extraction followed by gas chromatography (GC) or high-performance liquid chromatography are traditional herbicide residue determination methods for environmental samples. Solid-phase microextraction (SPME) is a solventless, fast, and sensitive alternative herbicide residue extraction method that can be
O Suzuki et al.
Forensic science international, 46(3), 169-180 (1990-07-01)
Positive-ion electron impact (PIEI), positive-ion chemical ionization (PICI) and negative-ion chemical ionization (NICI) mass spectra of 9 carbamate pesticides are presented. In the PIEI mode, the spectra showed small molecular peaks, intense or base peaks due to M - CH3NHCO
Luisito Cercaci et al.
Journal of chromatography. A, 985(1-2), 211-220 (2003-02-13)
The sterol composition of extra virgin olive oil is very characteristic and, thus, has become a helpful tool to detect adulterations with other vegetable oils. Special attention has been addressed to the separate determination of the free and esterified sterol
J M Jurado et al.
Talanta, 106, 14-19 (2013-04-20)
4-Methylsterols and 4,4-dimethylsterols of 47 samples of subcutaneous fat from Iberian pigs reared on two different fattening systems, "Extensive" and "Intensive", have been analyzed by GC-MS and GC-FID. The lipids were extracted by melting the subcutaneous fat in a microwave

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