G005910

LC/MS Analysis of Illicit Bath Salts on Ascentis^® Express HILIC, Set 1

application for HPLC

Eigenschaften

• Methode(n): HPLC: suitable
• Testparameter: column: Ascentis Express HILIC, 10 cm x 2.1 mm I.D., 2.7 μm particles (53939-U); mobile phase: 5 mM ammonium formate in [A] acetonitrile; [B] water; (98:2, A:B); flow rate: 0.6 mL/min; pressure: 267 psi (18.4 bar); column temp.: 35 °C; detector: MS, ESI(+) TOF, Summed Ion Chromatogram; injection: 2 μL; sample: 500 ng/mL in acetonitrile
• Eignung: application for HPLC
• Anwendung(en): forensics and toxicology

Beschreibung

Hinweis zur Analyse

HILIC mode operation on an Ascentis Express column provided baseline resolution of these bath salts, including isobaric compounds. The highest quality LC-MS solvents were used to supply low background interference and low particulate contaminants for robust, trouble-free operation. Cerilliant CRMs provided reliable identification and quantification.

Rechtliche Hinweise

Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyt

Naphyrone hydrochloride, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant^®
Pentylone hydrochloride, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant^®
MDPBP hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant^®
3-Methoxymethcathinone hydrochloride, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant^®
Methedrone hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant^®