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Merck

E-086

Supelco

3-epi-25-Hydroxyvitamin D3 solution

50 μg/mL in ethanol, certified reference material, Cerilliant®

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About This Item

Fórmula empírica (notación de Hill):
C27H44O2
Número de CAS:
Peso molecular:
400.64
MDL number:
UNSPSC Code:
12352205
PubChem Substance ID:
NACRES:
NA.24

grade

certified reference material

Quality Level

form

liquid

feature

Snap-N-Spike®/Snap-N-Shoot®

packaging

ampule of 1 mL

manufacturer/tradename

Cerilliant®

concentration

50 μg/mL in ethanol

mp

-144.0 °C

application(s)

clinical testing
clinical testing

format

single component solution

storage temp.

−20°C
−70°C

SMILES string

C[C@H](CCCC(C)(C)O)[C@H]1CC[C@H]2\C(CCC[C@]12C)=C\C=C3\C[C@H](O)CCC3=C

InChI

1S/C27H44O2/c1-19-10-13-23(28)18-22(19)12-11-21-9-7-17-27(5)24(14-15-25(21)27)20(2)8-6-16-26(3,4)29/h11-12,20,23-25,28-29H,1,6-10,13-18H2,2-5H3/b21-11+,22-12-/t20-,23-,24-,25+,27-/m1/s1

InChI key

JWUBBDSIWDLEOM-UEGFJKGBSA-N

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General description

A Certified Spiking Solution® of 3-epi-25-Hydroxyvitamin D3, the epi isomer of the prohormone 25-hydroxyvitamin D3. The presence of 3-epi-25-hydroxyvitamin D3 can affect accurate quantitation of 25-hydroxyvitamin D3 levels by most routine LC-MS/MS methods and to an unknown extent in immuno- and protein binding assays. This solution standard is suitable for critical quantitative applications in research and clinical environments including: for use in preparation of controls and calibrators for LC/UV and LC-MS/MS assays; as system tuning/suitability standards; linearity verification; internal proficiency testing; and for OEM use in preparation of reagents, development of assays and instrument IQ/OQ.

Application

3-epi-25-Hydroxyvitamin D3 may be used as a certified reference material (CRM) for the determination of the analyte in biological fluids by different chromatography techniques.

Legal Information

CERILLIANT is a registered trademark of Merck KGaA, Darmstadt, Germany
CERTIFIED SPIKING SOLUTION is a registered trademark of Cerilliant Corporation
Snap-N-Shoot is a registered trademark of Cerilliant Corporation
Snap-N-Spike is a registered trademark of Merck KGaA, Darmstadt, Germany

Related product

Referencia del producto
Descripción
Precios

pictograms

FlameExclamation mark

signalword

Danger

hcodes

Hazard Classifications

Eye Irrit. 2 - Flam. Liq. 2

Storage Class

3 - Flammable liquids

wgk_germany

WGK 1

flash_point_f

57.2 °F - closed cup

flash_point_c

14.0 °C - closed cup


Certificados de análisis (COA)

Busque Certificados de análisis (COA) introduciendo el número de lote del producto. Los números de lote se encuentran en la etiqueta del producto después de las palabras «Lot» o «Batch»

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A Method for Simultaneous Determination of 25-Hydroxyvitamin D3 and Its 3-Sulfate in Newborn Plasma by LC/ESI-MS/MS after Derivatization with a Proton-Affinitive Cookson-Type Reagent
Higashi T, et al.
Mass Spectrom., 5(2), S0051-S0051 (2016)
Measurement of serum 3-epi-25-hydroxyvitamin D3, 25-hydroxyvitamin D3 and 25-hydroxyvitamin D2 in infant, paediatric and adolescent populations of Korea using ultra-performance liquid chromatography-tandem mass spectrometry
Cho SE, et al.
Annals of Clinical Biochemistry, 54(5), 530-538 (2017)
Determination of four sulfated vitamin D compounds in human biological fluids by liquid chromatography--tandem mass spectrometry
Gomes FP, et al.
Journal of Chromatography. B, Biomedical Sciences and Applications, 1009(5), 80-86 (2016)

Artículos

This application shows an Ascentis Express F5 provided rapid resolution of the isobaric vitamin D metabolites. MS detection provides the necessary secondary resolution.

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