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G005273

US EPA Method 8100: GC Analysis of Polynuclear Aromatic Hydrocarbons (PAHs) on SLB®-5ms

suitable for GC

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About This Item

technique(s)

gas chromatography (GC): suitable

test parameters

column: SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
oven: 80 °C (2 min), 15 °C/min to 250 °C, 8 °C/min to 300 °C (5 min)
inj. temp.: 300 °C
MSD interface: 300 °C
scan range: m/z 40 - 450
carrier gas: helium, 1.2 mL/min constant
injection: 0.5 μL splitless (1 min)
liner: 2 mm I.D., FocusLiner™ with taper
sample: each analyte at 10 μg/mL in methylene chloride

application(s)

environmental

Legal Information

FocusLiner is a trademark of SGE Analytical Science Pty Ltd.
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

Description
    Naphthalene
    Acenaphthylene
    Acenaphthene
    Fluorene
    Phenanthrene
    Anthracene
    Carbazole
    Fluoranthene
    Pyrene
    Chrysene
    Benzo[b]fluoranthene
    Benzo[j]fluoranthene
    Benzo[k]fluoranthene
    Benzo[a]pyrene
    3-Methylcholanthrene
    Dibenz[a,h]acridine
    Dibenz[a,j]acridine
    Benzo[ghi]perylene
    Dibenzo(a,e)pyrene
    Dibenzo[a,i]pyrene
    Dibenzo[a,h]pyrene
    See All (21)

accessory

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Description
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analytical column

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Description
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guard column

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Description
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recommended

Product No.
Description
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required but not provided

Product No.
Description
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standard

Product No.
Description
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BCR266

7H-Dibenzo[c,g]carbazole, BCR®, certified reference material

BCR133

Dibenzo[a,e]pyrene, BCR®, certified reference material

BCR153R

Dibenz[a,h]acridine, BCR®, certified reference material

442506

Carbazole, analytical standard

48722-U

2-Fluorobiphenyl solution, 2000 μg/mL in dichloromethane, analytical standard

502332

Benzo[j]fluoranthene solution, certified reference material, 2000 μg/mL in dichloromethane

CRM48905

Polynuclear Aromatic Hydrocarbons Mix, certified reference material, TraceCERT®, 2000 μg/mL each component in methylene chloride: benzene (1:1)

CRM48743

EPA 610 Polynuclear Aromatic Hydrocarbons Mix, certified reference material, in methanol: methylene chloride (1:1) (varied concentration)

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