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Merck

HPLC Analysis of Tricyclic Antidepressants on Ascentis® ES Cyano

HPLC Analysis of Tricyclic Antidepressants on Ascentis® ES Cyano application for HPLC

材料

分析柱

產品號碼
描述
訂價

Ascentis® ES-CN HPLC 色谱柱

5 μm particle size, L × I.D. 15 cm × 4.6 mm

標準

產品號碼
描述
訂價

阿米替林盐酸盐标准液 盐酸盐 溶液

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

N-Desmethyldoxepin-D3 hydrochloride solution

cis/trans, 100 μg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

去甲丙咪嗪盐酸盐标准液 盐酸盐 溶液

1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

盐酸多塞平标准液 盐酸盐 溶液

1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

丙咪嗪标准液 CRM 盐酸盐 溶液

1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

去甲替林盐酸盐标准液 盐酸盐 溶液

1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

普罗替林 盐酸盐

1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

CONDITIONS

column

Ascentis ES Cyano, 15 cm x 4.6 mm I.D., 5 μm particles (577306-U)

mobile phase

[A] 10 mM potassium phosphate dibasic, pH 7 with phosphoric acid; [B] acetonitrile; [C] methanol; (25:60:15, A:B:C)

flow rate

2 mL/min

column temp.

25 °C

detector

UV, 215 nm

injection

5 μL

sample

100 μg/mL in water: methanol (70:30)

描述

分析報告

This application demonstrates the suitability of Ascentis ES Cyano for the efficient separation of tricyclic antidepressants.

法律資訊

Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany