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Merck

GC Analysis of FAMEs in Human Plasma on SLB®-IL111

GC Analysis of FAMEs in Human Plasma on SLB®-IL111 suitable for GC

材料

分析柱

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SLB®-IL111毛细管GC色谱柱

L × I.D. 100 m × 0.25 mm, df 0.20 μm

標準

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脂肪酸甲酯色谱柱评估混标

certified reference material, 1000 μg/mL each component in dichloromethane

相關產品

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三氟化硼-甲醇 溶液

~10% (~1.3 M), for GC derivatization, LiChropur

CONDITIONS

column

SLB-IL111, 100 m x 0.25 mm I.D., 0.20 μm (29647-U)

oven

50 ºC (4 min), 8 ºC/min to 160 °C (25 min), 4 ºC/min to 220 ºC

inj. temp.

230 °C

detector

FID, 240 ºC

carrier gas

hydrogen, 40 cm/sec

injection

2 μL 10:1 split

sample

FAMEs from 500 μL human plasma transesterified in sodium methoxide/methanol + boron trifluoride

描述

法律資訊

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany