技術
gas chromatography (GC): suitable
測試參數
column: Astec CHIRALDEX B-TA, 30 m x 0.25 mm I.D., 0.12 μm (73023AST)
gradient: 80 °C, 2 °C/min to 110 °C
inj. temp.: 250 °C
detector: FID, 250 °C
carrier gas: helium, 30 psi
injection: 0.6 μL, 80:1 split
sample: 2.5 mg/mL each racemate in methanol (N-TFA derivatives)
應用
chemicals and industrial polymers
法律資訊
Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC
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