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55286-U

Supelco

Supel QuE

PSA/C18/ENVI-Carb Tube, pk of 50, AOAC® 2007.01

同義詞:

QuEChERS

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About This Item

分類程式碼代碼:
41115712
NACRES:
NB.21

agency

AOAC® 2007.01

成份

Discovery® DSC-18, 400 mg
ENVI-Carb, 400 mg
magnesium sulfate, 1200 mg
Supelclean PSA, 400 mg

包裝

pk of 50

技術

QuEChERS: suitable

離心管體積

12 mL , Greiner Cat. No. 163270

應用

food and beverages

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一般說明

分散SPE法,通常也是指"QuEChERS” 方法(快速,简便,便宜,有效,耐用和安全),是一种现代样本准备技术,正在越来越多地被用在食品和农业产品多残基杀虫剂分析领域。

使用QuEChERS方法,食品/农产品样本首先在水溶性溶剂(比如乙腈),在高盐(比如氯化钠和硫酸镁)和或者缓冲试剂(比如柠檬酸盐)存在下,进行提取。高盐能够引起液相分离,而缓冲试剂能够稳定酸碱不稳定杀虫剂。 在摇晃和离心之后,有机相部分就进一步用SPE清洁。 和传统的SPE管方法不同,在分散SPE中,清洁需要混合大量的SPE(比如Supelclean PSA, ENVI-Carb, 和或者Discovery DSC-18)和提取物。 在样本清洁后,混合物经过离心,得到的上清可以直接分析,或者在分析前需要很少的处理。

Supelco有一系列的管和离心管,含有预置量的盐和SPE吸附剂,能够支持现今最常用的方法。

法律資訊

AOAC is a registered trademark of AOAC International
Discovery is a registered trademark of Merck KGaA, Darmstadt, Germany
Supel is a trademark of Sigma-Aldrich Co. LLC

儲存類別代碼

11 - Combustible Solids

水污染物質分類(WGK)

WGK 3

閃點(°F)

Not applicable

閃點(°C)

Not applicable


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Stanisław Walorczyk
Talanta, 120, 106-113 (2014-01-29)
A triple quadrupole GC-QqQ-MS/MS method was optimized for multiresidue analysis of over 180 pesticides in blackcurrants. The samples were prepared by using a modified quick, easy, cheap, effective, rugged and safe (QuEChERS) analytical protocol. To reduce matrix co-extractives in the
Determination of toxic substances, pesticides and mycotoxins, in ginkgo biloba nutraceutical products by liquid chromatography Orbitrap-mass spectrometry
Martinez-Dominguez, G., et al.
Microchemical Journal, Devoted to the Application of Microtechniques in All Branches of Science, 118, 124-130 (2015)
Chun-Lin Fan et al.
Journal of AOAC International, 98(1), 130-148 (2015-04-11)
A 3 month study was conducted on the ruggedness of a multiresidue method for accuracy and stability. The results indicate that in terms of Youden pair ratios of 201 pesticide aged tea samples falling approximately within 1.00-1.20 of the ratio
Tsuyoshi Imazawa et al.
Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan, 46(6), 277-281 (2006-01-31)
An analytical method was developed for the determination of phenmedipham (PM) in agricultural products using reversed-phase high-performance liquid chromatography with UV detection. A sample was extracted with acetonitrile, and the acetonitrile layer was separated by salting-out. The acetonitrile phase was
U Führer et al.
Analytical and bioanalytical chemistry, 354(3), 333-343 (1996-01-01)
Halogenated anisoles (methyl-phenyl ethers) appear to be ubiquitous organic trace compounds in the environment. An analytical method is presented for analyzing the altogether 134 congeners of chloro-, bromo- and mixed bromochloro-anisoles on an isomer-specific basis in air. High volume sampling

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