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Key Documents

8.55003

Sigma-Aldrich

Rink Amide MBHA树脂(100-200目)

Novabiochem®

同義詞:

Rink Amide MBHA树脂(100-200目)

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About This Item

CAS號碼:
分類程式碼代碼:
12352111
NACRES:
NA.22

品質等級

產品線

Novabiochem®

形狀

beads

反應適用性

reaction type: Fmoc solid-phase peptide synthesis

製造商/商標名

Novabiochem®

應用

peptide synthesis

官能基

amine

儲存溫度

2-30°C

一般說明

该支持物包括通过正亮氨酸连接至MBHA树脂的修饰的Rink酰胺接头,并且是肽酰胺Fmoc SPP的理想工具。可以通过用95% TFA进行单步处理来实现从该树脂的裂解,从而以高收率和纯度提供肽酰胺。

相关方案和技术文章
肽合成用树脂的上样方案

應用


  • Liquid chromatography-tandem mass spectrometry for forensic analysis: LSD-D₃ is utilized as an internal standard in the liquid chromatography-tandem mass spectrometry determination of LSD and its metabolites in forensic samples, enhancing accuracy and precision in the analytical results (Johansen and Jensen, 2005).

  • Isotope dilution mass spectrometry in urine testing: Employed in the high-performance liquid chromatography-isotope dilution mass spectrometry (IDMS) method, LSD-D₃ serves as a crucial internal standard for the quantification of lysergide (LSD) in urine, aiding in precise and accurate drug testing (White et al., 1999).

  • Automated extraction and LC/MS/MS confirmation: LSD-D₃ is used in the automated extraction of lysergic acid diethylamide from various biological matrices, followed by confirmation using LC/MS/MS. This application highlights its role in improving the efficiency and reliability of toxicological analyses (de Kanel et al., 1998).

聯結

替代品:01-64-0037

分析報告

颜色(目测):白色至浅黄色至米黄色
物质外观(目测):微珠
负载量(光度法测定DBU/DMF处理后释放的Fmoc生色团):0.40 - 0.90 mmol/g
TNBS检验:符合检验
溶胀体积(DMF):结果因批次而异
溶胀体积(CH₂Cl₂):结果因批次而异
根据Houben Weyl得到的总溶胀体积(CH2Cl2): ≥ 5.2 ml/g
根据Houben Weyl得到的总溶胀体积(DMF): ≥ 5.2 ml/g
聚合物基质为共聚物(苯乙烯-1% DVB),100 - 200目。

法律資訊

Novabiochem is a registered trademark of Merck KGaA, Darmstadt, Germany

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儲存類別代碼

11 - Combustible Solids

水污染物質分類(WGK)

WGK 3

閃點(°F)

Not applicable

閃點(°C)

Not applicable


分析證明 (COA)

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文章

Novabiochem® has one of the most extensive ranges of linkers and derivatized resins for Fmoc solid phase peptide synthesis. These resins have varied properties with special protocols for loading and cleaving.

Novabiochem® has one of the most extensive ranges of linkers and derivatized resins for Fmoc solid phase peptide synthesis. These resins have varied properties with special protocols for loading and cleaving.

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