1.05794

TLC plates, Silica gel 60 F₂₅₄

pkg of 100 plates, plate L × W 2.5 cm × 7.5 cm, glass support

• 同義詞: Silica Gel 60 F₂₅₄ TLC Plates
• 分類程式碼代碼: 41115711
• NACRES: NB.21

屬性

• 材料: glass support; silica gel 60 matrix
• 品質等級: 100
• 特點: binder Organic Polymer; fluorescent indicator
• 包裝: pkg of 100 plates
• 技術: thin layer chromatography (TLC): suitable
• 層厚度: 250 μm
• 板長度 × 寬度: 2.5 cm × 7.5 cm
• 粒徑: 10-12 μm
• 孔徑: 60 Å medium pore diameter
• 儲存溫度: 2-30°C

描述

一般說明

100 Glass plates 2,5 x 7,5 cm

應用

• MSTFA as an Effective TMS Source for the TMSOTf-Catalyzed Synthesis of Cyclic Acetals: This study demonstrates the utility of 2,2,2-Trifluoro-N-methyl-N-(trimethylsilyl)acetamide as an effective trimethylsilyl donor in the synthesis of cyclic acetals, showcasing its role in facilitating catalyst efficiency and improving reaction conditions for organic synthesis within the realm of green chemistry practices (Radomkit et al., 2024).

聯結

Replaces: 15341-1; 15341

分析報告

Specific surface area (according to BET; 5-Pt.measurement): 480 - 540 m²/g
Pore volume(N₂-isotherm):0.74 - 0.84 ml/g
d 50 (laserdiffraction, size distribution): 9.7 - 11.7 µm
Layerthickness: 210 - 270 µm
Deviationof layer thickness per plate: ≤ 35 µm
Chromatographictesting:
A) colourtest
hRf-values
- bleu viforganol, lipophile: 11 - 25
- CeresBlack G, lipophile: 34 - 48
- ceresViolet brn, lipophile: 52 - 67
separationnumber (colour test, lipophile): ≥ 10.5
B)Steroid test
hRf-values
- Hydrocortisone, steroid test: 25 - 37
- Reichstein S, steroid test: 37 - 49
- Methyltestosterone, steroid test: 42 - 54
Typical value determined on a conditioned plate
Eluent A) Toluene (45% rel. humidity)
Eluent B) Ethyl acetate/Toluene (95+5 v/v; 20% rel. humidity)