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G005105

GC Analysis of 5-Amino-1,3,3-Trimethylcyclohexanemethylamine Enantiomers (N-TFA Derivatives) on Astec® CHIRALDEX™ A-TA

suitable for GC

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technique(s)

gas chromatography (GC): suitable

test parameters

column: Astec CHIRALDEX A-TA, 30 m x 0.25 mm I.D., 0.12 μm (73003AST)
oven: 160 °C
inj. temp.: 250 °C
detector: FID, 250 °C
carrier gas: helium, 30 psi
injection: 1 μL, 80:1 split
sample: 3 mg/mL racemate in methanol
peaks 1 & 2: first enantiomer pair
peaks 3 & 4: second enantiomer pair

application(s)

chemicals and industrial polymers

Legal Information

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC

analytical column

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standard

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