技術
HPLC: suitable
測試參數
column: Ascentis Express Phenyl-Hexyl, 10 cm x 2.1 mm I.D., 2.7 μm particles (53336-U)
mobile phase: [A] water, acetonitrile, 90:10; [B] acetonitrile
gradient: 0% B held for 0.5 min; to 15% B in 1 min; held at 15% B for 6 min
flow rate: 0.3 mL/min
pressure: 192 bar (2780 psi)
column temp.: 30 °C
detector: UV, 218 nm
injection: 10 μL
sample: 5 mg/L ea. in 95:5, water:acetonitrile
適合性
application for HPLC
應用
agriculture
food and beverages
分析報告
The trichothecene vomitoxins of Fusarium are significant plant pathogens of grain and forage crops that can lead to anorexic effects with livestock. This application demonstrates resolution of deoxynivalenol and three of its analogs.
法律資訊
Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany
分析物
说明
Nivalenol hydrate
15-Acetyldeoxynivalenol solution
3-Acetyldeoxynivalenol
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