技術
gas chromatography (GC): suitable
solid phase microextraction (SPME): suitable
測試參數
SPME fiber: polydimethylsiloxane phase fiber, 100 μm headspace sampling (20 min) 10 sec desorption (splitless mode) (57300-U)
column: 100% methyl polysiloxane, 30 m × 0.25 mm I.D., 0.25 μm (Supelco equivalent, Equity-1, 28046-U)
oven: 35 °C (2 min) to 220 °C at 10 °C/min, hold 2 min, to 300 °C at 30 °C/min, hold 5 min
inj. temp.: splitless (closed 3 min), 220 °C (2 mm I.D. injector liner)
detector: FID, 300 °C
carrier gas: helium, 1 mL/min (split 50:1)
適合性
application for SPME
應用
forensics and toxicology
分析物
说明
m-Xylene
p-Xylene
Naphthalene
Toluene
Ethylbenzene
o-Xylene
1,2,3-Trimethylbenzene
1,2,4-Trimethylbenzene
2-Methylnaphthalene
1-Methylnaphthalene
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