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agency
suitable for USP L8
品質等級
特點
endcapped
製造商/商標名
SUPELCOSIL™
標籤範圍
3% Carbon loading
參數
≤70 °C temp. range
400 bar pressure (5801 psi)
技術
HPLC: suitable
長度 × 內徑
25 cm × 4.6 mm
表面積
170 m2/g
表面覆盖率
surface coverage 5.1 μmol/m2
基質
silica gel, spherical particle platform
基質活性組
amino phase
粒徑
5 μm
孔徑
120 Å
應用
food and beverages
分離技術
hydrophilic interaction (HILIC)
normal phase
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一般說明
氨基柱最常用于分离单糖和二糖。作为正相应用,氨基塔可用于石油工业(参见SUPELCOSIL™ LC-NH2-NP HPLC色谱柱章节,以了解更多详情)。
硅胶基质的 SUPELCOSIL LC-NH2 色谱柱分离单糖、二糖和一些三糖时其出峰顺序通常是,随分子量的增大化合物保留时间延长。随着水:乙腈在流动相中的比例增大,保留时间减小。更多信息请参阅 T397126(SUPELCOSIL LC-NH2 色谱柱中的糖)。
法律資訊
SUPELCOSIL is a trademark of Sigma-Aldrich Co. LLC
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Food chemistry, 217, 346-351 (2016-09-25)
An analytical method was developed and validated for the determination of maltodextrin in raw milk, using high-performance liquid chromatography with evaporative light scattering detection. Maltodextrin content was evaluated in adulterated raw milk using a Supelcosil LC-NH2 (25cm×4.6mm) column and isocratic
Utilization of Lactobacillus sp. for steroid glycoalkaloids degradation by lactic acid fermentation.
Die Nahrung, 46(4), 251-255 (2002-09-13)
The degradation fo steroid glycoalkaloids (SGAs) has been studied in model solutions. The number of colony forming units (CFU) was determined using a nondirect (cultivation) method during all stages of fermentation. The changes in SGAs content were observed by HPLC
Journal of chromatography. A, 1119(1-2), 238-245 (2005-12-21)
Ibuprofen arginate is a rapidly absorbed salt designed to promote more rapid onset of analgesia than commercially available forms of ibuprofen. Ibuprofen and arginine have very different polarities and this becomes in a chromatographic problem, further complicated with the determination
实验方案
HPLC Analysis of Sugars on SUPELCOSIL™ LC-NH2
Chromatograms
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