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54182-U

Supelco

Supel™-Select HLB SPE 小柱

bed wt. 60 mg, volume 3 mL, pk of 50

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About This Item

分類程式碼代碼:
41115712
NACRES:
NB.21

材料

PE frit (20 μm)
polypropylene hardware

品質

MS friendly

成份

bed wt., 60 mg

包裝

pk of 50

技術

solid phase extraction (SPE): suitable

表面積

160-420 m2/g

容積

3 mL

基質

Hydrophilic modified styrene polymer particle platform

基質活性組

polystyrene phase

粒徑

50-70 μm

孔徑

80-200 Å pore size

應用

food and beverages

分離技術

reversed phase

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一般說明

保留机制：反相
样品基质相容性：水溶液（生物流体、水）

  • 亲水改性苯乙烯聚合物
  • 开发用于从水样中提取多种化合物
  • 保留主要基于反相；然而，由于该相是亲水改性的，它也适用于极性化合物。
  • 被保留和回收的更具极性的化合物的例子包括（但不限于）： 吡哆醇（logPo/w -0.56）、核黄素（logPo/w -2.02）、生物素（logPo/w 0.11）。

應用

Supel™-Select HLB SPE管可用作萃取柱柱体，用于固相萃取，运用液相色谱电喷雾电离串联质谱法测定水样品中的抗生素。

特點和優勢

  • 价格低，样品制备性能出色
  • 适合通用方法 - 在方法开发过程中节省时间、金钱和令人头痛的事
  • 更大的容量允许更小的床重 = 更小的洗脱体积 = 节省样品处理时间
  • 抗过度干燥，可使用更强的方法
  • 低 UV 和 MS 可萃取物，可降低背景并提高灵敏度
  • 严格的生产和 QC 指南提供更高的批次间、管间和井间一致性，以提高准确性和精密度

法律資訊

Supel is a trademark of Sigma-Aldrich Co. LLC

儲存類別代碼

11 - Combustible Solids

水污染物質分類（WGK）

WGK 3

閃點（°F）

Not applicable

閃點（°C）

Not applicable

从最新的版本中选择一种：

分析证书(COA)

Lot/Batch Number
14827901
14698601
14519801
14428101
14334701

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Analysis of selected antibiotics in surface freshwater and seawater using direct injection in liquid chromatography electrospray ionization tandem mass spectrometry
Bayen S, et al.
Journal of Chromatography A, 1338, 38-43 (2014)
Chiedza F Munyeza et al.
Biomedical chromatography : BMC, 30(6), 837-845 (2015-09-18)
Tigecycline (TIG), a derivative of minocycline, is the first in the novel class of glycylcyclines and is currently indicated for the treatment of complicated skin structure and intra-abdominal infections. A selective, accurate and reversed-phase high-performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS)
Pablo Vazquez-Roig et al.
Analytical and bioanalytical chemistry, 397(7), 2851-2864 (2010-05-01)
A simple and robust method using solid-phase extraction (SPE) and liquid chromatography tandem mass spectrometry (LC-MS/MS) for the simultaneous determination of 14 drugs of abuse and their metabolites (cocainics, amphetamine-like compounds, cannabinoids, and opiates) in surface waters has been developed.
Wei Chen et al.
Chemosphere, 163, 99-107 (2016-08-16)
A sensitive method for simultaneous determination of 20 trace organic chemicals (TOrCs, including preservatives, antioxidants, disinfectants, oestrogens, alkyl-phenols and bisphenol-A) in surface water and wastewater has been developed and validated based on the optimisation of solid-phase extraction (SPE) followed by
Martina Rejtharová et al.
Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment, 34(4), 477-481 (2016-12-06)
Monitoring of steroid esters in blood serum is desirable in order to detect the possible illegal use of natural hormones as growth promoters. A method for the determination of testosterone propionate, testosterone benzoate, testosterone isocaproate, testosterone decanoate and estradiol benzoate

商品

Supel-Select HLB SPE for Pharmaceutical Analysis

Select HLB SPE is a hydrophilic polymer phase for analyte extraction from aqueous matrices. Here it’s used for statins in plasma and 48 pharmaceutical analytes in drinking water.

Supel-Select HLB SPE for Pharmaceutical Analysis

Select HLB SPE is a hydrophilic polymer phase for analyte extraction from aqueous matrices. Here it’s used for statins in plasma and 48 pharmaceutical analytes in drinking water.

Solid Phase Extraction: Reversed-Phase Methodology

Reversed-phase interaction will retain most molecules with hydrophobic character; it is very useful for extracting analytes that are very diverse in structure within the same sample.

Solid Phase Extraction: Reversed-Phase Methodology

Reversed-phase interaction will retain most molecules with hydrophobic character; it is very useful for extracting analytes that are very diverse in structure within the same sample.

实验方案

LC MS Analysis of Triclosan Irgasan in Waste Water

Separation of Irgasan, ≥97.0% (HPLC)

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