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產品線
Novabiochem®
化驗
≥98% (TLC)
≥98.0% (HPLC)
形狀
powder
反應適用性
reaction type: Boc solid-phase peptide synthesis
製造商／商標名
Novabiochem®
應用
peptide synthesis
儲存溫度
15-25°C
InChI
1S/C18H23N3O6S/c1-12-5-7-14(8-6-12)28(25,26)21-10-13(19-11-21)9-15(16(22)23)20-17(24)27-18(2,3)4/h5-8,10-11,15H,9H2,1-4H3,(H,20,24)(H,22,23)/t15-/m0/s1
InChI 密鑰
DCLJSEPKYJSEHW-HNNXBMFYSA-N
一般說明
Standard building block for introduction of histidine amino-acid residues by Boc SPPS.
Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Boc SPPS
Literature references
[1] T. Fujii, et al. (1974) Bull. Chem. Soc. Jpn., 47, 3146.
[2] J. M. v. d. Eijk, et al. (1980) J. Org. Chem., 45, 547.
Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Boc SPPS
Literature references
[1] T. Fujii, et al. (1974) Bull. Chem. Soc. Jpn., 47, 3146.
[2] J. M. v. d. Eijk, et al. (1980) J. Org. Chem., 45, 547.
聯結
Replaces: 04-12-0012
分析報告
Colour (visual): white to slight yellow to beige
Appearance of substance (visual): powder
Identity (IR): passes test
Optical rotation α 25/D (c=1 in dioxan): +10.0 - +13.0 °
Purity (TLC(011B)): ≥ 98 %
Purity (TLC(011C)): ≥ 98 %
Assay (HPLC, area%): ≥ 98.0 % (a/a)
Solubility (50 mg in ml EtOH): clearly soluble
To see the solvent systems used for TLC of Novabiochem® products please click here.
Appearance of substance (visual): powder
Identity (IR): passes test
Optical rotation α 25/D (c=1 in dioxan): +10.0 - +13.0 °
Purity (TLC(011B)): ≥ 98 %
Purity (TLC(011C)): ≥ 98 %
Assay (HPLC, area%): ≥ 98.0 % (a/a)
Solubility (50 mg in ml EtOH): clearly soluble
To see the solvent systems used for TLC of Novabiochem® products please click here.
法律資訊
Novabiochem is a registered trademark of Merck KGaA, Darmstadt, Germany
儲存類別代碼
11 - Combustible Solids
水污染物質分類（WGK）
WGK 3
閃點（°F）
Not applicable
閃點（°C）
Not applicable
实验方案
The most popular reagent for cleavage of peptides from Boc-based resins is anhydrous HF. Of all the cleavage procedures HF appears to be the most versatile and least harmful to a wide variety of peptides synthesized on Boc-based resins.
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