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Merck
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Key Documents

1.05620

Supelco

TLC Silica gel 60 F₂₅₄ Multiformat prescored to 5 x 10 cm

pkg of 25 plates, plate L × W 20 cm × 20 cm, glass support

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About This Item

分類程式碼代碼:
41115711
NACRES:
NB.21

材料

glass support
silica gel 60 matrix

品質等級

特點

binder Organic Polymer
fluorescent indicator

包裝

pkg of 25 plates

技術

thin layer chromatography (TLC): suitable

板長度 × 寬度

20 cm × 20 cm

尺寸

250 μm

粒徑

10-12 μm

孔徑

60 Å medium pore diameter

儲存溫度

2-30°C

一般說明

25 Glass plates 20 x 20 cm,
These pre-scored glass plates fold into smaller formats with just one easy snap of the fingers.

應用

Glass TLC plate, silica gel coated with flourescent indicator F254. The silica gel TLC plates come in a quantity of 25 size 20x20 cm for thin layer chromatography applications.

聯結

Replaces: 105620-7; 105620

分析報告

Specific surface area (according to BET; 5-Pt. measurement): 480 - 540 m²/g
Pore volume (N₂-isotherm): 0.74 - 0.84 ml/g
d 50 (laser diffraction, size distribution): 9.7 - 11.7 µm
Layer thickness: 210 - 270 µm
Deviation of layer thickness per plate: ≤ 35 µm
Chromatographic testings:
A) Colour test
hRf-values
- bleu vif organol, colour test, lipophile:
11 - 25
- Ceres Black G, colour test, lipophile: 34 - 48
- ceres Violet brn, colour test, lipophile: 52 - 67
separation number (colourtest, lipophile): ≥ 10.5
B) Steriod test
hRf-values
- hydrocortisone, steroid test:
25 - 37
- Reichstein S, steroid test: 37 - 49
- methyltestosterone, steroid test: 42 - 54
Typical value determined on a conditioned plate
Eluent A) Toluene (45% rel.humidity)
Eluent B) Ethyl acetate/Toluene (95+5 v/v; 20% rel.humidity)

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