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化驗
97%
形狀
liquid
折射率
n20/D 1.6570 (lit.)
bp
133-134 °C/10 mmHg (lit.)
mp
−2-−1 °C (lit.)
密度
1.48 g/mL at 20 °C (lit.)
SMILES 字串
Brc1cccc2ccccc12
InChI
1S/C10H7Br/c11-10-7-3-5-8-4-1-2-6-9(8)10/h1-7H
InChI 密鑰
DLKQHBOKULLWDQ-UHFFFAOYSA-N
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一般說明
1-溴萘可用作交叉偶联反应合成联芳基化合物的中间体。
應用
1-溴萘一种溴代芳烃，可用于：
- 与芳基三氟硼酸的钯催化Suzuki–Miyaura偶联反应，无需相转移催化剂或膦配体。
- 通过Suzuki-Heck型偶联，与o-溴苯基硼酸和寡环溴芳烃反应，制备Indeno环并多环芳烃。
- 与PhMgBr的Ni催化Kumada–Tamao–Corriu 交叉偶联反应。
- 通过与芳基硼酸的钯催化Suzuki-Miyaura交叉偶联反应制备芳基萘。
訊號詞
Warning
危險聲明
危險分類
Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Eye Irrit. 2
儲存類別代碼
10 - Combustible liquids
水污染物質分類（WGK）
WGK 3
閃點（°F）
230.0 °F - closed cup
閃點（°C）
110 °C - closed cup
個人防護裝備
Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter
其他客户在看
High efficiency of cavity-based triaryl-phosphines in nickel-catalysed Kumada-Tamao-Corriu cross-coupling
Monnereau L, et al.
Chemical Communications (Cambridge, England), 47(23), 6626-6628 (2011)
Microwave-accelerated Suzuki-Miyaura coupling reactions using potassium aryltrifluoroborates
Harker RL and Crouch RD
Synthesis, 2007(01), 25-27 (2007)
A New Suzuki- Heck-Type Coupling Cascade: Indeno [1, 2, 3]-Annelation of Polycyclic Aromatic Hydrocarbons
Wegner HA, et al.
The Journal of Organic Chemistry, 68(3), 883-887 (2003)
Exploring the selectivity of the Suzuki-Miyaura cross-coupling reaction in the synthesis of arylnaphthalenes
Lima CFRAC, et al.
Tetrahedron, 67(4), 689-697 (2011)
Xin-zhen Du et al.
Guang pu xue yu guang pu fen xi = Guang pu, 24(4), 402-406 (2005-03-16)
Room-temperature phosphorescence of 1-BrN induced by a combination of OPE-10 and Triton X-100 with beta-CD was comparatively studied. In terms of molecular size and dimensions of beta-CD, the octyl group and phenyl group of OPE-10 and Triton X-100 were incorporated
实验方案
Zirconium bromonorbornanelactone carboxylate triacrylate (PRM30) is a zirconium-containing multifunctional acrylate useful for producing cured, transparent films with high refractive indices.
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