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反應適用性
reaction type: Grignard Reaction
品質等級
濃度
0.5 M in THF
bp
65 °C (lit.)
密度
0.960 g/mL at 25 °C (lit.)
官能基
chloro
儲存溫度
2-8°C
SMILES 字串
Clc1cccc([Mg]Br)c1
InChI
1S/C6H4Cl.BrH.Mg/c7-6-4-2-1-3-5-6;;/h1-2,4-5H;1H;/q;;+1/p-1
InChI 密鑰
ZIYRUWPTUPFRQU-UHFFFAOYSA-M
應用
3-Chlorophenylmagnesium bromide (o-chlorophnylmagnesium bromide) is a Grignard reagent that can be used to synthesize:
- 2,3-Di(o-chlorophenyl)buta-1,3-dienes by reacting with 1,4-dimethoxy 2-butyne in the presence of a copper(I) salt.
- 2-Bromo-5-chlorothiophen-3-yl-(3-chlorophenyl)methanol by reacting with 2-bromo-5-chlorothiophene-3-carbaldehyde.
- 2-(3-Chlorophenyl)-1-phenyl-1H-inden-1-ol from 2- benzoylbenzonitrile as a starting a material.
法律資訊
Rieke® Metals, Inc. 产品 ®Rieke Metals, Inc. 的注册商标
訊號詞
Danger
危險分類
Acute Tox. 4 Oral - Carc. 2 - Eye Irrit. 2 - Flam. Liq. 2 - STOT SE 3
標靶器官
Respiratory system
安全危害
儲存類別代碼
3 - Flammable liquids
水污染物質分類(WGK)
WGK 3
閃點(°F)
<1.4 °F - closed cup
閃點(°C)
< -17 °C - closed cup
The discovery of 4-1-[({2, 5-dimethyl-4-[4-(trifluoromethyl) benzyl]-3-thienyl}carbonyl) amino] cyclopropyl}benzoic acid (MK-2894), a potent and selective prostaglandin E2 subtype 4 receptor antagonist
Journal of Medicinal Chemistry, 53(5), 2227-2238 (2010)
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