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同位素純度
99.8 atom % D
品質等級
化驗
≥99.00%
形狀
liquid
包含
0.1 % (v/v) TMS
技術
NMR: suitable
雜質
≤0.0100% water
water
折射率
n20/D 1.444 (lit.)
bp
60.9 °C (lit.)
mp
−64 °C (lit.)
密度
1.500 g/mL at 25 °C (lit.)
質量偏移
M+1
SMILES 字串
[2H]C(Cl)(Cl)Cl
InChI
1S/CHCl3/c2-1(3)4/h1H/i1D
InChI 密鑰
HEDRZPFGACZZDS-MICDWDOJSA-N
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一般說明
Chloroform-d (deuterochloroform, CDCl3) is a deuterated NMR solvent containing 0.1 % (v/v) TMS (tetramethylsilane). It is useful in NMR-based research and analyses. It may be synthesized by reacting trichloroacetophenone and sodium deuteroxide. The influence of the number of pulses on its multiphoton decomposition (MPD) has been studied. Infrared spectral studies of C-D stretching and bending motions of CDCl3 in different solvents have been investigated. The effect of chloroform-d on the interaction of water with activated carbons has been analyzed. The dependence of molecular reorientation of deuterated chloroform on pressure and temperature has been studied by Raman spectroscopy.
應用
Chloroform-d may be used in the synthesis of dichlorofluoromethane-d.
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訊號詞
Danger
危險分類
Acute Tox. 3 Inhalation - Acute Tox. 4 Oral - Carc. 2 - Eye Irrit. 2 - Repr. 2 - Skin Irrit. 2 - STOT RE 1 Oral - STOT SE 3
標靶器官
Central nervous system, Liver,Kidney
儲存類別代碼
6.1D - Non-combustible acute toxic Cat.3 / toxic hazardous materials or hazardous materials causing chronic effects
水污染物質分類(WGK)
WGK 3
閃點(°F)
Not applicable
閃點(°C)
Not applicable
個人防護裝備
Eyeshields, Faceshields, Gloves
其他客户在看
Isotope Effect on Dissociation Probabilities in the Mass Spectra of Chloroform and Chloroform-d.
J. Chem. Phys., 19(4), 404-406 (1951)
The effect of collisions in the multiphoton decomposition of chloroform-d.
J. Chem. Phys. , 92(10), 5997-6003 (1990)
Influence of organics on the structure of water adsorbed on activated carbons.
Journal of Colloid and Interface Science, 253(1), 23-34 (2002)
Raman study of molecular reorientation in liquid chloroform and chloroform-d under high pressure.
J. Chem. Phys. , 69(12), 5479-5488 (1978)
Dichlorofluoromethane-d: a versatile solvent for VT-NMR experiments.
The Journal of Organic Chemistry, 53(11), 2629-2630 (1988)
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