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GC Analysis of Amphetamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX™ G-DP

GC Analysis of Amphetamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX™ G-DP suitable for GC

Materials

Analytical column

Product No.
Description
Pricing

78033AST

Astec® CHIRALDEX™ G-DP Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.12 μm

Application

Product No.
Description
Pricing

G005053

GC Analysis of Amphetamine Enantiomers (N-Trifluoroacetyl Derivative) on Astec® CHIRALDEX™ G-PN

suitable for GC

Standard

Product No.
Description
Pricing

A3278

D-Amphetamine hemisulfate salt solution

1.0 mg/mL in methanol, analytical standard, for drug analysis

A1263

DL-Amphetamine sulfate salt

A5880

D-Amphetamine hemisulfate salt

94777

DL-Amphetamine hydrochloride

analytical standard

CONDITIONS

column

Astec CHIRALDEX G-DP, 30 m x 0.25 mm I.D., 0.12 μm (78033AST)

oven

140 °C

detector

FID, 250 °C

inj. temp.

250 °C

carrier gas

helium, 2.7 mL/min., constant flow

injection

1 μL, 80:1 split

liner

4 mm I.D., FocusLiner

sample

4 mg/mL each compound in methylene chloride
peak 1: d-amphetamine (N-TFA derivative)
peak 2: l-amphetamine (N-TFA derivative)

Description

Analysis Note

Elution order reversal (l,d) by using CHIRALDEX G-PN, 130°C (see G005053).

Legal Information

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC

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