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Key Documents

G003577

US EPA Method 8270: GC Analysis of Semivolatiles on SLB®-5ms, 350 °C Final Oven Temp.

suitable for GC

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About This Item

technique(s)

gas chromatography (GC): suitable

test parameters

column: SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
oven: 40 °C (3 min), 20 °C/min to 100 °C, 15 °C/min to 200 °C, 30 °C/min to 350 °C (3 min)
inj. temp.: 250 °C
MSD interface: 350 °C
scan range: m/z 40-450
carrier gas: helium, ramped flow, 1 mL/min. (8 min), 10 mL/min2 to 1.5 mL/min (hold for remainder of run)
injection: 0.5 μL splitless (0.3 min)
liner: 2 mm I.D., straight
sample: 25 ng on-column of a 72 component semivolatile standard and 8 surrogates, plus 6 internal standards (at 20 ng on-column)

application(s)

environmental

Analysis Note

Typical run times for US EPA Method 8270 range from 23 to 45 minutes. In this application, the high maximum operating temperature of the SLB-5ms was utilized to reduce run time to < 19 minutes.

Legal Information

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

Description
    N-Nitrosodimethylamine
    Pyridine
    2-Fluorophenol
    Aniline
    Phenol-d6
    Phenol
    Bis(2-chloroethyl) ether
    2-Chlorophenol
    1,3-Dichlorobenzene
    1,4-Dichlorobenzene
    Benzyl alcohol
    1,2-Dichlorobenzene
    o-Cresol
    Bis-(2-chloroisopropyl) ether
    N-Nitrosodi-n-propylamine
    p-Cresol
    Hexachloroethane
    Nitrobenzene-d5
    Nitrobenzene
    Isophorone
    2-Nitrophenol
    2,4-Dimethylphenol
    Bis(2-chloroethoxy)methane
    Benzoic acid
    2,4-Dichlorophenol
    1,2,4-Trichlorobenzene
    Naphthalene
    4-Chloroaniline
    4-Chloro-3-methylphenol
    2-Methylnaphthalene (β)
    Hexachlorocyclopentadiene
    2,4,6-Trichlorophenol
    2,4,5-Trichlorophenol
    2-Fluorobiphenyl
    2-Chloronaphthalene
    2-Nitroaniline
    Dimethyl phthalate
    2,6-Dinitrotoluene
    Acenaphthylene
    3-Nitroaniline
    Acenaphthene
    Dibenzofuran
    2,4-Dinitrotoluene
    Diethyl phthalate
    Fluorene
    4-Chlorodiphenyl ether
    4-Nitroaniline
    2-Methyl-4,6-dinitrophenol
    N-Nitrosodiphenylamine
    Azobenzene
    4-Bromodiphenyl ether
    Hexachlorobenzene
    Pentachlorophenol
    Phenanthrene
    Anthracene
    Carbazole
    Fluoranthene
    Benzidine
    Pyrene
    o-Tolidine
    3,3′-Dichlorobenzidine
    Bis(2-ethylhexyl) phthalate
    Chrysene
    Di-n-octyl phthalate
    Benzo[b]fluoranthene
    Benzo[k]fluoranthene
    Benzo[a]pyrene
    Benzo[ghi]perylene
    See All (68)

analytical column

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