335614
3-Chloropropiophenone
98%
Sinónimos:
β-Chloropropiophenone, 3-Chloro-1-phenyl-1-propanone
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About This Item
Productos recomendados
assay
98%
form
solid
bp
113-115 °C/4 mmHg (lit.)
mp
48-50 °C (lit.)
functional group
chloro
SMILES string
ClCCC(=O)c1ccccc1
InChI
1S/C9H9ClO/c10-7-6-9(11)8-4-2-1-3-5-8/h1-5H,6-7H2
InChI key
KTJRGPZVSKWRTJ-UHFFFAOYSA-N
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Application
3-Chloropropiophenone was used in the asymmetric reduction of (S)-3-chloro-1-phenylpropanol using preheated Candida utilis cells immobilized in calcium alginate gel beads. It was also used in the synthesis of (R)-3-chloro-1-phenyl-1-propanol via asymmetric reduction using in-situ generated oxazaborolidine catalyst derived from (S)-α,α-diphenylprolinol.
Storage Class
11 - Combustible Solids
wgk_germany
WGK 3
flash_point_f
Not applicable
flash_point_c
Not applicable
ppe
Eyeshields, Gloves, type N95 (US)
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Asymmetric Synthesis of (R)-Fluoxetine: A Practical Approach Using Recyclable and in-situ Generated Oxazaborolidine Catalyst.
Chin. J. Chem., 27(6), 1137-1140 (2009)
Biotechnology letters, 31(12), 1879-1883 (2009-07-28)
An efficient method for asymmetric reduction of (S)-3-chloro-1-phenylpropanol from 3-chloropropiophenone was developed using preheated Candida utilis cells immobilized in calcium alginate gel beads. Heating the immobilized cells (bead diameter 1.5 mm) at 45 degrees C for 50 min allowed the
Journal of drug targeting, 25(9-10), 796-808 (2017-07-21)
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Styrene monooxygenase (SMO) can catalyze the kinetic resolution of secondary allylic alcohols to provide enantiopure glycidol derivatives. To overcome the low theoretical yield of kinetic resolution, we designed a one-pot two-step enzymatic cascade using prochiral α,β-unsaturated ketones as the substrates.
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