186317
N,N-Diethylformamide
99%
Synonym(s):
N-Formyldiethylamine
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About This Item
Linear Formula:
HCON(C2H5)2
CAS Number:
Molecular Weight:
101.15
Beilstein:
1209392
EC Number:
MDL number:
UNSPSC Code:
12352100
PubChem Substance ID:
NACRES:
NA.22
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Quality Level
Assay
99%
form
liquid
refractive index
n20/D 1.434 (lit.)
bp
176-177 °C (lit.)
density
0.908 g/mL at 25 °C (lit.)
SMILES string
CCN(CC)C=O
InChI
1S/C5H11NO/c1-3-6(4-2)5-7/h5H,3-4H2,1-2H3
InChI key
SUAKHGWARZSWIH-UHFFFAOYSA-N
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General description
N,N-Diethylformamide undergoes condensation with aromatic o-aminonitriles in the presence of ZnCl2 in sealed reactor to yield quinazoline-2,4(1H,3H)-dione.
Application
N,N-Diethylformamide was used in the synthesis of metal-organic frameworks. It was also used as solvent in the synthesis of porous cubic-shaped ZnO particles.
Signal Word
Warning
Hazard Statements
Precautionary Statements
Hazard Classifications
Eye Irrit. 2 - Flam. Liq. 3 - Skin Irrit. 2 - STOT SE 3
Target Organs
Respiratory system
WGK
WGK 1
Personal Protective Equipment
dust mask type N95 (US), Eyeshields, Gloves
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A new and facile preparation of quinazoline-2,4(1H,3H)-diones was first reported which was the condensation of aromatic o-aminonitriles with DMF or N,N-diethylformamide in the presence of ZnCl(2) (0.5-10 mol %) at 190-200 degrees C in the sealed reactor.
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