GC Analysis of 2,5-Dimethoxytetrahydrofuran Enantiomers on Astec^® CHIRALDEX^™ G-TA

column

Astec CHIRALDEX G-TA, 30 m x 0.25 mm I.D., 0.12 μm (73033AST)

oven

70 °C

inj. temp.

250 °C

detector

FID, 250 °C

carrier gas

helium, 30 psi

injection

0.2 μL, 80:1 split

sample

2 mg/mL in ethanol
peaks 1 & 2: 2,5-dimethoxytetrahydrofuran enantiomers
peak 3: meso-isomer