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Merck

GC Analysis of 1-Methyl-3-Phenylpropylamine (4-Phenyl-2-Butylamine) Enantiomers (N-TFA Derivatives) on Astecยฎ CHIRALDEXโ„ข G-TA

GC Analysis of 1-Methyl-3-Phenylpropylamine (4-Phenyl-2-Butylamine) Enantiomers (N-TFA Derivatives) on Astec® CHIRALDEX™ G-TA suitable for GC

Materials

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Astecยฎ CHIRALDEXโ„ข G-TA Capillary GC Column

L ร— I.D. 30 m ร— 0.25 mm, df 0.12 ฮผm

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1-Methyl-3-phenylpropylamine

98%

CONDITIONS

column

Astec CHIRALDEX G-TA, 30 m x 0.25 mm I.D., 0.12 μm (73033AST)

oven

130 ยฐC

inj. temp.

250 ยฐC

detector

FID, 250 ยฐC

carrier gas

helium, 30 psi

sample

peaks 1 & 2: 1-methyl-3-phenylpropylamine (4-phenyl-2-butylamine) enantiomers (N-TFA derivatives)

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Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC