G005799

GC Analysis of Pesticides in Beef Kidney on SLB^®-5ms (20 m x 0.18 mm I.D., 0.36 μm) after QuEChERS Cleanup using Supel^™ Que Z-Sep+, MS in SIM Mode, Fast GC Analysis

suitable for GC, application for SPE

속성

• 기술: gas chromatography (GC): suitable; solid phase extraction (SPE): suitable
• 검사 파라미터: sample preparation: Dispersive (QuEChERS); sample/matrix: 10 gm homogenized beef kidney spiked at 50 ng/g with pesticides; extraction tube: Supel Que Acetate (AC) Tube (55234-U); extraction process: add 10 mL of acetonitrile; shake for 1 minute; add contents of Supel Que acetate extraction tube (55234-U); shake immediately for 1 minute; centrifuge at 3200 rpm for 5 minutes; (Sample Pretreatment: Homogenize 10 gm beef kidney and spike with pesticides at 50 ng/g.); clean-up tube: Supel QuE Z-Sep+ tube (55296-U); clean-up process: transfer 3 mL of the acetonitrile layer into a Supel QuE Z-Sep+ cleanup tube (55296-U); shake for 1 minute; centrifuge at 3400 rpm for 3 minutes; draw off supernatant for LVI-GCMS analysis; column: F.S. CAP. SLB-5MS 20 m x 0.18 mm I.D., 0.36 μm (28576-U); oven: 70 °C ( 0.5 min), 25 °C/min to 125 °C, 10 °C/min to 200 °C, 5 °C/min to 300 °C/min (1 min); inj. temp.: programmed, 60 °C (0.28 min), 600 °C/min to 325 °C (5 min); detector: MSD; MSD interface: 325 °C; carrier gas: helium, 1 mL/min constant flow; injection: 10 μL LVI, PTV solvent vent, rapid injection speed; liner: 4 mm ID FocusLiner with taper; sample: Beef Kidney extract
• 적합성: application for SPE
• 응용 분야: food and beverages

설명

분석 메모

Beef kidney was analyzed for pesticides by GC/MS-SIM after extraction and cleanup. Dispersive SPE was used for both extraction and cleanup. Since beef kideny contains approximately 5% fat, Z-Sep + was used for cleanup.

법적 정보

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

Supel is a trademark of Sigma-Aldrich Co. LLC

분석물

Diphenylamine
Hexachlorobenzene
Lindane
Endosulfan I
4,4′-DDE
1,1-Dichloro-2,2-bis(4-chlorophenyl)ethane
Endosulfan sulfate
4,4′-DDT
Piperonylbutoxide
Bifenthrin
Permethrin (isomers) solution
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