797-0627

GC Analysis of Fragrance Compounds in Shampoo Base on a 100% Methyl Column after SPME using 100 μm PDMS Fiber

suitable for GC, application for SPME

속성

• 기술: gas chromatography (GC): suitable; solid phase microextraction (SPME): suitable
• 검사 파라미터: SPME fiber: polydimethylsiloxane, 100 μm film (57300-U); extraction: headspace, 5 min, 80 °C (with sample stirring); desorption process: 5 min, 250 °C; desorption temp.: -50 °C w/liquid CO₂; column: 100% methyl polysiloxane, 50 m × 0.25 mm I.D., 0.25 μm (Supelco equivalent, Equity-1, 28047-U); oven: 35 °C to 240 °C at 3 °C/min; inj. temp.: split, 250 °C; detector: MSD, scan m/z = 29-350 AMU; carrier gas: helium, 0.5 mL/min; sample: 0.5 g shampoo base with 1% fragrance test mix, diluted 1:1 with NaCl/water in a 10 mL vial
• 적합성: application for SPME
• 응용 분야: cleaning products; cosmetics; personal care

분석물

Menthol
Methyl salicylate
Eugenol
(R)-(+)-Limonene, purum, ≥98.0% (sum of enantiomers, GC)
Benzyl acetate
Myrcene
Linalool
Linalyl acetate
Benzyl salicylate
Citronellol
(±)-Citronellal
(−)−α-Terpineol, natural, ≥96%, FCC, FG
α-Hexylcinnamaldehyde, ≥95%, stabilized, FG
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