추천 제품
material
polypropylene tube
Quality Level
Agency
suitable for EN 15662
제품 라인
Supel™
구성
magnesium sulfate, 4 g
sodium chloride, 1 g (Cat. No. S7653)
sodium citrate dibasic sesquihydrate, 0.5 g (Cat. No. 71635)
sodium citrate tribasic dihydrate, 1 g (Cat. No. S4641)
포장
pk of 50
기술
QuEChERS: suitable
원심분리 튜브 용적
15 mL
응용 분야
food and beverages
분리 기술
ion exchange
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일반 설명
Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.
Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.
애플리케이션
적합성
법적 정보
애플리케이션
Storage Class Code
13 - Non Combustible Solids
WGK
WGK 1
Flash Point (°F)
Not applicable
Flash Point (°C)
Not applicable
Choose from one of the most recent versions:
문서
Compared to conventional PSA/C18/GCB cleanup, cannabis extracts cleaned with the Supel QuE Verde mixture showed lower GC/MS background, and better recoveries for many pesticides.
Pistachios contain approximately 45% fat, which can result in a significant amount of coextracted matrix in the acetonitrile extract generated using the QuEChERS procedure. A zirconia based adsorbent significantly reduces coextracted matrix prior to LC-MS or GC-MS.
A procedure for cleanup of green tea extracts provides low background and allowed for the analysis of more pesticides at lower levels than QuEChERS. Uses less solvents and no toluene.
A procedure for cleanup of green tea extracts provides low background and allowed for the analysis of more pesticides at lower levels than QuEChERS. Uses less solvents and no toluene.
프로토콜
A highly selective and sensitive analytical method was developed for chloramphenicol using a QuEChERS type sample preparation approach and LC-MS/MS detection.
LC/MS/MS Analysis of Pesticide Residues in Pistachios on the Ascentis® Express RP-Amide Column after QuEChERS Extraction
관련 콘텐츠
QuEChERS is a ‘Quick, Easy, Cheap, Effective, Rugged and Safe’ sample cleanup method used to prepare food and agricultural samples for pesticides analysis. QuEChERS is based on the Solid Phase Extraction (SPE) technique of sample preparation.
QuEChERS method simplifies sample cleanup for pesticides analysis in food and agricultural samples.
Solid phase extraction purifies samples for chromatographic analysis, improving data quality and protecting analytical columns.
Chromatograms
application for HPLCapplication for HPLC, application for SPE자사의 과학자팀은 생명 과학, 재료 과학, 화학 합성, 크로마토그래피, 분석 및 기타 많은 영역을 포함한 모든 과학 분야에 경험이 있습니다..
고객지원팀으로 연락바랍니다.