추천 제품
product name
Astec® CYCLOBOND I 2000 HP-RSP Chiral HPLC Column, 5 μm particle size, L × I.D. 15 cm × 4.6 mm
material
stainless steel column
Quality Level
제품 라인
Astec®
포장
pkg of 1 ea
제조업체/상표
Astec®
파라미터
0-50 °C temperature
172 bar pressure (2500 psi)
기술
HPLC: suitable
LC/MS: suitable
길이 × I.D.
15 cm × 4.6 mm
기질
silica particle platform
fully porous particle
기질 활성군
cyclodextrin, beta- phase
입자 크기
5 μm
공극 크기
100 Å
작동 pH
3.5-7
분리 기술
chiral
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일반 설명
In the design of this new chemistry, it was an objective to create a very stable and reproducible phase with shorter retention times, while maintaining or improving selectivity over CYCLOBOND I 2000 RSP. With that goal and more achieved, CYCLOBOND I 2000 HP-RSP separates by extended H-bonding capability, and offers broad chiral selectivity for chiral screening. It is most beneficial for basic and neutral compounds.
- Bonded phase: (R,S)-Hydroxypropyl modified β-cyclodextrin (high performance)
법적 정보
Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
Assessment of the complexation degree of camptothecin derivatives and cyclodextrins using spectroscopic and separative methodologies
Foulon, C., et al.
Tetrahedron Asymmetry, 20 (21), 2482-2489 (2009)
Reprint of: Enantiomeric separation of functionalized ethano-bridged Troger bases using macrocyclic cyclofructan and cyclodextrin chiral selectors in high-performance liquid chromatography and capillary electrophoresis with application of principal component analysis
Weatherly, Choyce A., et al.
Journal of Chromatography. B, Biomedical Applications, 968, 40-48 (2014)
High-performance liquid chromatographic enantioseparation of bicalutamide and its related compounds.
Roland Török et al.
Journal of chromatography. A, 1098(1-2), 75-81 (2005-11-30)
Direct high-performance liquid chromatographic methods were developed for the enantioseparation of (R,S)-bicalutamide (1) and its analogs (+/-)-3-chloro-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide (2), (+/-)-N-(4-cyano-3-(trifluoro-methyl)phenyl)-2-methyloxirane-2-carboxamide (3), (+/-)-4-fluorophenylsulfonyl-2-hydroxy-2-methylpropionic acid (4) and (+/-)-3-hydroxy-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide (5). The methods involved the use of a cellulose-based Chiralcel OD-H, macrocyclic glycopeptide-based Chirobiotic T
Xinxin Han et al.
Journal of chromatography. A, 1063(1-2), 111-120 (2005-02-11)
The enantiomeric separation of a set of 30 new chiral furan derivatives has been achieved on native and derivatized beta-cyclodextrin stationary phases using high performance liquid chromatography (HPLC). The hydroxypropyl-beta-cyclodextrin (Cyclobond RSP), the 2,3-dimethyl-beta-cyclodextrin (Cyclobond DM), and the acetyl-beta-cyclodextrin (Cyclobond
관련 콘텐츠
CYCLOBOND is the name given to Astec technology for bonding cyclodextrins to a high purity silica gel through a stable ether linkage.
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