1.05794

TLC plates, Silica gel 60 F₂₅₄

pkg of 100 plates, plate L × W 2.5 cm × 7.5 cm, glass support

• 동의어(들): Silica Gel 60 F₂₅₄ TLC Plates
• UNSPSC 코드: 41115711
• NACRES: NB.21

속성

• material: glass support; silica gel 60 matrix
• Quality Level: 100
• 특징: binder Organic Polymer; fluorescent indicator
• 포장: pkg of 100 plates
• 기술: thin layer chromatography (TLC): suitable
• 레이어 두께: 250 μm
• 플레이트 길이 × 너비: 2.5 cm × 7.5 cm
• 입자 크기: 10-12 μm
• 공극 크기: 60 Å medium pore diameter
• 저장 온도: 2-30°C

설명

일반 설명

100 Glass plates 2,5 x 7,5 cm

애플리케이션

• MSTFA as an Effective TMS Source for the TMSOTf-Catalyzed Synthesis of Cyclic Acetals: This study demonstrates the utility of 2,2,2-Trifluoro-N-methyl-N-(trimethylsilyl)acetamide as an effective trimethylsilyl donor in the synthesis of cyclic acetals, showcasing its role in facilitating catalyst efficiency and improving reaction conditions for organic synthesis within the realm of green chemistry practices (Radomkit et al., 2024).

결합

Replaces: 15341-1; 15341

분석 메모

Specific surface area (according to BET; 5-Pt.measurement): 480 - 540 m²/g
Pore volume(N₂-isotherm):0.74 - 0.84 ml/g
d 50 (laserdiffraction, size distribution): 9.7 - 11.7 µm
Layerthickness: 210 - 270 µm
Deviationof layer thickness per plate: ≤ 35 µm
Chromatographictesting:
A) colourtest
hRf-values
- bleu viforganol, lipophile: 11 - 25
- CeresBlack G, lipophile: 34 - 48
- ceresViolet brn, lipophile: 52 - 67
separationnumber (colour test, lipophile): ≥ 10.5
B)Steroid test
hRf-values
- Hydrocortisone, steroid test: 25 - 37
- Reichstein S, steroid test: 37 - 49
- Methyltestosterone, steroid test: 42 - 54
Typical value determined on a conditioned plate
Eluent A) Toluene (45% rel. humidity)
Eluent B) Ethyl acetate/Toluene (95+5 v/v; 20% rel. humidity)