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G003894

GC Analysis of Closely Eluting Analytes from US EPA Method 8270 on SLB®-5ms (30 m x 0.25 mm I.D., 0.25 μm)

suitable for GC

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technique(s)

gas chromatography (GC): suitable

test parameters

column: SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
oven: 40 °C (2 min), 22 °C/min to 240 °C, 10 °C/min to 330 °C (1 min)
inj. temp.: 250 °C
detector: FID, 330 °C
carrier gas: helium, 30 cm/sec @ 200 °C, set using methane
injection: 0.5 μL splitless (0.75 min)
liner: 4 mm I.D., single taper
sample: 50 ng on-column of a 72 component semivolatile standard and 8 surrogate compounds, plus 6 internal standards (at 40 ng on-column), in methylene chloride

application(s)

environmental

Legal Information

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

Description
    Benzo[b]fluoranthene
    Benzo[k]fluoranthene
    Benzo[a]pyrene
    Perylene-d12
    Indeno[1,2,3-c,d]pyrene solution
    Benzo[ghi]perylene

analytical column

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