55227-U
Supel™ QuE
Citrate Extraction Tube, pk of 50, suitable for EN 15662
Synonym(s):
QuEChERS
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About This Item
UNSPSC Code:
41115712
NACRES:
NB.21
material
polypropylene tube
Quality Level
Agency
suitable for EN 15662
product line
Supel™
composition
magnesium sulfate, 4 g
sodium chloride, 1 g (Cat. No. S7653)
sodium citrate dibasic sesquihydrate, 0.5 g (Cat. No. 71635)
sodium citrate tribasic dihydrate, 1 g (Cat. No. S4641)
packaging
pk of 50
technique(s)
QuEChERS: suitable
centrifuge tube volume
15 mL
application(s)
food and beverages
separation technique
ion exchange
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General description
Dispersive SPE (dSPE), often referred to as the "QuEChERS" method (Quick, Easy, Cheap, Effective, Rugged, and Safe), is modern sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.
Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.
Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.
Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.
Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.
Application
Supel™ QuE citrate tube is used for the determination of pesticide residues on vegetables using various analytical techniques.
Suitability
Suitable for extracting ~10 g food/agricultural sample. The citrate is to buffer the extraction to pH 5.0 - 5.5. At this pH, most acid and base labile pesticides are stable.
Legal Information
Supel is a trademark of Sigma-Aldrich Co. LLC
Storage Class Code
13 - Non Combustible Solids
WGK
WGK 1
Flash Point(F)
Not applicable
Flash Point(C)
Not applicable
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