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Key Documents

G005092

GC Analysis of Alkylamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX™ B-TA

suitable for GC

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About This Item

technique(s)

gas chromatography (GC): suitable

test parameters

column: Astec CHIRALDEX B-TA, 30 m x 0.25 mm I.D., 0.12 μm (73023AST)
gradient: 80 °C, 2 °C/min to 110 °C
inj. temp.: 250 °C
detector: FID, 250 °C
carrier gas: helium, 30 psi
injection: 0.6 μL, 80:1 split
sample: 2.5 mg/mL each racemate in methanol (N-TFA derivatives)

application(s)

chemicals and industrial polymers

Legal Information

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC

analytical column

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standard

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