Skip to Content
Merck
All Photos(1)

Key Documents

More Documents

55439-U

Supelco

Supel™ QuE

PSA/C18 Tube (Shaker Compatible), pk of 50, suitable for EN 15662:2008 per BS, centrifuge tube volume 15 mL , Shaker Compatible

Synonym(s):

QuEChERS

Sign Into View Organizational & Contract Pricing
All Photos(1)

About This Item

UNSPSC Code:
41115712
NACRES:
NB.21

material

polypropylene tube

Quality Level

100

Agency

suitable for BS EN 15662:2008

product line

Supel™

composition

Discovery® DSC-18, 150 mg (Cat. No. 52600-U)
Magnesium Sulfate, 900 mg
Supelclean™ PSA, 150 mg (Cat. No. 52738-U)

packaging

pk of 50

technique(s)

QuEChERS: suitable

centrifuge tube volume

15 mL , Shaker Compatible

matrix active group

C18 phase
PSA phase

application(s)

food and beverages

Looking for similar products? Visit Product Comparison Guide

Related Categories

General description

Dispersive SPE (dSPE), often referred to as the "QuEChERS" method (Quick, Easy, Cheap, Effective, Rugged, and Safe), is modern sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.

Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.

Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.

Compatibility

Compatible with most QuEChERS shakers.

Suitability

Suitable for food/agricultural samples of higher fat content. Ideal for clean up of 6 mL extract after initial food extraction and phase partitioning.

Legal Information

Discovery is a registered trademark of Merck KGaA, Darmstadt, Germany
Supel is a trademark of Sigma-Aldrich Co. LLC
Supelclean is a trademark of Sigma-Aldrich Co. LLC

Storage Class Code

13 - Non Combustible Solids

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable

Choose from one of the most recent versions:

Certificates of Analysis (COA)

Lot/Batch Number
17118301
17003401
16868101
16715101
16398401

Don't see the Right Version?

If you require a particular version, you can look up a specific certificate by the Lot or Batch number.

Search for a COA

Already Own This Product?

Find documentation for the products that you have recently purchased in the Document Library.

Visit the Document Library

Customers Also Viewed

Slide 1 of 4

1 of 4

Supel™ QuE Z-Sep+ Tube, pk of 50, centrifuge tube volume 15 mL , Shaker Compatible

Supelco

55486-U

Supel™ QuE

Supelco

Supelco

55234-U

Supel™ QuE

Supelco

Supelco

55237-U

Supel™ QuE

Supel™ QuE Verde Tube, centrifuge tube volume 15 mL, pack of 50 ea

Supelco

55442-U

Supel™ QuE Verde

Steven J Lehotay et al.
Journal of chromatography. A, 1217(16), 2548-2560 (2010-02-11)
This article describes the comparison of different versions of an easy, rapid and low-cost sample preparation approach for the determination of pesticide residues in fruits and vegetables by concurrent use of gas and liquid chromatography (GC and LC) coupled to
Lijun Han et al.
Analytica chimica acta, 827, 40-46 (2014-05-17)
A new method of sample preparation was developed and is reported for the first time. The approach combines in-vial filtration with dispersive solid-phase extraction (d-SPE) in a fast and convenient cleanup of QuEChERS (quick, easy, cheap, effective, rugged, and safe)
M Picot Groz et al.
The Science of the total environment, 493, 162-169 (2014-06-20)
The UV filters and musk fragrances have come into focus because these compounds are contained and increasingly used not only in sunscreen products but also in many products of daily use, such as cosmetics, skin creams, plastics or varnish. In
Maria Teresa Salles Trevisan et al.
Journal of chromatography. A, 1512, 98-106 (2017-07-20)
An analytical method using a quick, easy, cheap, effective, rugged and safe (QuEChERS) procedure for multi-residue determination of 52 pesticides in coffee leaf extractshas been developed and validated according to SANTE/11945/2015 guidelines. Different sorbent combinations for dispersive solid phase extraction
David Moreno-González et al.
Talanta, 128, 299-304 (2014-07-26)
In this study a fast, selective and sensitive multiresidue method based on QuEChERS methodology has been evaluated and validated for the determination of carbamate pesticides, in edible vegetable oils by UHPLC-MS/MS. A new clean-up sorbent, Supel(TM) QuE Z-Sep(+), has been
View All Related Papers

Related Content

QuEChERS Sample Preparation Method

QuEChERS is a ‘Quick, Easy, Cheap, Effective, Rugged and Safe’ sample cleanup method used to prepare food and agricultural samples for pesticides analysis. QuEChERS is based on the Solid Phase Extraction (SPE) technique of sample preparation.

QuEChERS Sample Prep Method

QuEChERS method simplifies sample cleanup for pesticides analysis in food and agricultural samples.

Our team of scientists has experience in all areas of research including Life Science, Material Science, Chemical Synthesis, Chromatography, Analytical and many others.

Contact Technical Service