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P-097

Supelco

Psilocybin solution

1.0 mg/mL in acetonitrile: water (1:1), ampule of 1 mL, certified reference material, Cerilliant®

Synonym(s):

3-[2-(Dimethylamino)ethyl]-1H-indol-4-yl phosphate solution

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About This Item

Empirical Formula (Hill Notation):
C12H17N2O4P
CAS Number:
Molecular Weight:
284.25
EC Number:
UNSPSC Code:
41116107
NACRES:
NA.24

grade

certified reference material

Quality Level

form

liquid

feature

(Snap-N-Spike®)

packaging

ampule of 1 mL

manufacturer/tradename

Cerilliant®

drug control

Narcotic Licence Schedule D (Switzerland); psicótropo (Spain); Decreto Lei 15/93: Tabela IIA (Portugal)

concentration

1.0 mg/mL in acetonitrile: water (1:1)

technique(s)

gas chromatography (GC): suitable
liquid chromatography (LC): suitable

application(s)

forensics and toxicology

format

single component solution

storage temp.

−70°C

InChI

1S/C12H17N2O4P/c1-14(2)7-6-9-8-13-10-4-3-5-11(12(9)10)18-19(15,16)17/h3-5,8,13H,6-7H2,1-2H3,(H2,15,16,17)

InChI key

QVDSEJDULKLHCG-UHFFFAOYSA-N

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General description

This certified Snap-N-Spike® solution is suitable for a variety of GC/MS or LC/MS testing applications including for use in forensic analysis, urine drug testing, or clinical toxicology.

Psilocybin is a natural psychoactive compound that belongs to the class of tryptamine alkaloids. It is one of the main hallucinogenic compounds of widely known “magic mushrooms”― Psilocybe, Panaeolus, and Conocybe. Known by street names such as shrooms, boomers, or musk, psilocybin has effects similar to LSD and DMT.

Application

The certified reference solution (CRM) in solution can also be used as follows:
  • Simultaneous quantitative analysis of psilocybin, γ-hydroxybutyric acid, and ibotenic acid in human saliva samples using capillary electrophoresis (CE) along with a capacitively coupled contactless conductivity detector (C4D)
  • Development of an ultra-high-performance liquid chromatography-tandem mass spectrometric (UHPLC–MS/MS) method to quantify psilocybin and psilocin in samples of seized hallucinogenic mushrooms and hair obtained from accused users
  • Multi-residue analysis of psilocybin, mescaline, N,N-dimethyltryptamine, psilocin, and salvinorin A in human hair samples using ultra-high-pressure liquid chromatography (UHPLC) combined with tandem mass spectrometry (MS/MS)
  • Measurement of 11 multi-class illicit drugs in human urine and plasma samples by their micro-solid phase extraction (μSPE) followed by analysis by liquid chromatography-electrospray ionization-tandem mass spectrometry (LC-ESI-MS/MS)

Features and Benefits

  • Fully characterized under ISO/IEC 17025 and ISO 17034 accreditation
  • Accompanied with a comprehensive Certificate of Analysis (CoA) with data on stability, homogeneity, accuracy of concentration, uncertainty, and traceability
  • Rigorously tested through real-time stability studies to ensure accuracy and shelf life
  • Gravimetrically prepared using qualified precision balances to ensure minimal uncertainty
  • Flame sealed under argon into ampoules for long-term shelf life
  • Offered in a convenient, DEA-exempt format to improve laboratory efficiency

Recommended products

Find a digital Reference Material for this product available on our online platform ChemisTwin® for NMR. You can use this digital equivalent on ChemisTwin® for your sample identity confirmation and compound quantification (with digital external standard). An NMR spectrum of this substance can be viewed and an online comparison against your sample can be performed with a few mouseclicks. Learn more here and start your free trial.

Legal Information

CERILLIANT is a registered trademark of Merck KGaA, Darmstadt, Germany
Snap-N-Spike is a registered trademark of Merck KGaA, Darmstadt, Germany

Pictograms

FlameExclamation mark

Signal Word

Danger

Hazard Statements

Hazard Classifications

Acute Tox. 4 Oral - Eye Irrit. 2 - Flam. Liq. 2

Storage Class Code

3 - Flammable liquids

WGK

WGK 2

Flash Point(F)

42.8 °F - closed cup

Flash Point(C)

6.0 °C - closed cup


Certificates of Analysis (COA)

Search for Certificates of Analysis (COA) by entering the products Lot/Batch Number. Lot and Batch Numbers can be found on a product’s label following the words ‘Lot’ or ‘Batch’.

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Articles

The HPLC method was first optimized using a ginsenoside standard mixture and was then applied to a sample of American Ginseng root.

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