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Key Documents

G005071

GC Analysis of Amphetamine and Methamphetamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX™ G-PN

suitable for GC

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About This Item

technique(s)

gas chromatography (GC): suitable

test parameters

column: Astec CHIRALDEX G-PN, 30 m x 0.25 mm I.D., 0.12 μm (74033AST)
oven: 130 °C
detector: FID, 250 °C
inj. temp.: 250 °C
carrier gas: helium, 30 psi
injection: 1 μL, 80:1 split
sample: 3 mg/mL each compound in methanol
peak 1: d-methamphetamine
peak 2: l-methamphetamine
peak 3: l-amphetamine
peak 4: d-amphetamine

application(s)

clinical
forensics and toxicology
pharmaceutical (small molecule)

Analysis Note

Elution order reversal of amphetamine (d,l) by using CHIRALDEX G-DP, 140°C.

Legal Information

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC

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