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Key Documents

G004377

US EPA Method 608.1/608.2: GC Analysis of Organochlorine Pesticides on SPB®-608

suitable for GC

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technique(s)

gas chromatography (GC): suitable

test parameters

column: SPB-608, 30 m x 0.25 mm I.D., 0.25 μm (24103-U)
oven: 75 °C (2 min), 15 °C/min to 300 °C (5 min)
inj. temp.: 250 °C
detector: ECD, 300 °C
carrier gas: helium, 1.2 mL/min. constant
injection: 1 μL, splitless (splitter open after 0.75 min)
liner: 4 mm I.D., single taper
sample: mixture of 608.1 and 608.2 calibration solutions (40351-U and 40352-U) diluted to 100 ppb in n-hexane

application(s)

environmental

Legal Information

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

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