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Merck
  • Thiol-promoted catalytic synthesis of diphenolic acid with sulfonated hyperbranched poly(arylene oxindole)s.

Thiol-promoted catalytic synthesis of diphenolic acid with sulfonated hyperbranched poly(arylene oxindole)s.

Chemical communications (Cambridge, England) (2012-03-02)
Stijn Van de Vyver, Jan Geboers, Sasja Helsen, Feng Yu, Joice Thomas, Mario Smet, Wim Dehaen, Bert F Sels
摘要

Acid-catalyzed condensation of levulinic acid and phenol into high yields of diphenolic acid (>50%) is possible with a combination of sulfonated hyperbranched polymers and thiol promotors, either added as a physical mixture or bound to the polymer by ion-pairing.

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Sigma-Aldrich
乙酰丙酸, 98%
Sigma-Aldrich
乙酰丙酸, ≥97%, FG
Sigma-Aldrich
乙酰丙酸, natural, 99%, FG