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813066

TSKgel® Boronate-5PW HPLC Column

phase m-aminophenyl boronate, L × I.D. 7.5 cm × 7.5 mm, 10 μm particle size

Synonym(s):

TSKgel® Boronate-5PW HPLC Column

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About This Item

UNSPSC Code:
41115700

material

PEEK

product line

TSKgel®

analyte chemical class(es)

proteins

manufacturer/tradename

Tosoh Boronate-5PW, 13066

parameter

≤20% organic solvent
≤3 M salt concentration
1.2 mL/min flow rate
30 bar max. pressure
≥ 0 °C temperature

technique(s)

HPLC: suitable

L × I.D.

7.5 cm × 7.5 mm

matrix

polymer particle platform

matrix active group

m-aminophenyl boronate phase

particle size

10 μm

pore size

1000 Å

operating pH

2-9

capacity

40 μmol/mL adsorption capacity (sorbitol)

compatibility

mode of use affinity HPLC

separation technique

affinity

storage temp.

2-8°C

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General description

High efficiency, resin-based TSKgel affinity columns (10 μm particles) separate or purify many enzymes and other proteins.

Coupling of m-aminophenyl boronate to TSKgel 5PW polymeric support results in a ligand capable of forming a tetrahedral boronate anion under alkaline pH conditions. This anionic structure can bind with 1,2 cis-diol groups such as those found in carbohydrates, carbohydrate containing compounds and catecholamines. Interaction between the boronate anion and the 1,2 cis-diol groups is enhanced in the presence of Mg2+ ions and is inhibited by amine-containing buffers. Adsorption onto the TSKgel Boronate-5PW matrix takes place in basic buffers such as HEPES and morpholine while desorption takes place in carbohydrate or amine-containing mobile phase like sorbitol or Tris.

Applications include: nucleic acids, catecholamines, nucleosides and nucleotides.

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Legal Information

TSKgel is a registered trademark of Tosoh Corporation

Storage Class Code

10 - Combustible liquids

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable


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