575664-U
Supel™-Select SCX SPE 96-well Plate
bed wt. 30 mg/well, pk of 1
About This Item
Matériaux
PE frit (20 μm)
polypropylene hardware
Qualité
MS Friendly
Composition
bed wt., 30 mg/well
Conditionnement
pk of 1
Technique(s)
solid phase extraction (SPE): suitable
Superficie
160-420 m2/g
Matrice
Sulfonic acid functionalized hydrophilic modified styrene polymer particle platform
Groupe de la matrice active
sulfonic acid phase
Taille des particules
50-70 μm
Dimension de pores
80-200 Å pore size
Application(s)
food and beverages
Technique de séparation
ion exchange
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Description générale
Sample Matrix Compatibility: Aqueous solutions (biological fluids, water)
- Sulfonic acid functionalized hydrophilic modified styrene polymer
- Developed for the extraction of a highly broad range of compounds from aqueous samples
- Retention predominately based on ion-exchange; however, because the phase is hydrophilic modified, it is amenable to polar compounds as well.
Caractéristiques et avantages
- Excellent sample prep performance at a lower price
- Amenable to generic methodology - save time, money, and headache during method development
- Greater capacity allows for smaller bed weights = smaller elution volumes = time savings in sample processing
- Resistance to overdrying allows for more robust methdology
- Low UV and MS extractables for lower background and greater sensitivity
- Stringent production and QC guidelines offer greater lot-to-lot, tube-to-tube, and well-to-well consistency for improved accuracy and precision
Informations légales
Mention d'avertissement
Warning
Mentions de danger
Conseils de prudence
Classification des risques
Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
Organes cibles
Respiratory system
Code de la classe de stockage
11 - Combustible Solids
Classe de danger pour l'eau (WGK)
WGK 3
Point d'éclair (°C)
Not applicable
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Certificats d'analyse (COA)
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Articles
Shown here is the chiral separation of amphetamine enantiomers under MS-compatible conditions on Astec CHIROBIOTIC® V2 after extraction from urine using Supel™-Select SCX SPE 96-well plates. The highest grade mobile phase solvents and additives were used to supply low background interference and low particulate contaminants for robust, trouble-free operation. Cerilliant CRMs provided reliable identification and quantification.
SPE retention mechanism in this case is based on the electrostatic attraction of charged functional groups of the analyte(s) to oppositely charged functional groups on the sorbent.
Protocoles
In this study, optimized methods are presented for sample preparation and chiral chromatography for the LC/MS analysis of amphetamine and methamphetamine enantiomers in urine.
Optimized sample prep and chiral chromatography methods for the LC/MS analysis of these drug enantiomers in urine
LC/MS Analysis of Methamphetamine Enantiomers on Astec® CHIROBIOTIC® V2 in Urine after SPE using Supel™-Select SCX
Retention occurs through polar interaction between the sorbent and analytes. Typical sample matrices that can be employed in normal-phase SPE include hydrocarbon or fatty oils diluted in a solvent like hexane, isooctane, chlorinated solvent, THF, diethyl ether, or ethyl acetate.
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