LC/MS Analysis of Cocaine, Cocaethylene, Oxycodone, and Noroxycodone on Discovery® HS F5
Materiales
columna analítica
Referencia del producto
Descripción
Precios
patrón
Referencia del producto
Descripción
Precios
Cocaethylene solution
1.0 mg/mL in acetonitrile, ampule of 1 mL, certified reference material, Cerilliant®Noroxycodone hydrochloride solution
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®Oxycodone solution
1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®CONDITIONS
column
Discovery HS F5, 5 cm x 2.1 mm I.D., 3 μm particles (567500-U)
mobile phase
[A] 10 mM ammonium formate in water, pH 6.8; [B] 10mM ammonium formate in acetonitrile, pH 6.8; (10:90, A:B)
flow rate
0.3 mL/min
column temp.
35 °C
detector
ESI(+)
injection
2 μL
sample
200 ng/mL in 25:75, water:acetonitrile
Descripción
Información legal
Discovery is a registered trademark of Merck KGaA, Darmstadt, Germany