GC Analysis of Volatiles in Purple Nitrile Gloves on SPB®-HAP after Collection/Desorption using Carbotrap® 300 Tube
CONDITIONS
sample/matrix
0.5 g purple nitrile glove
thermal desorption tube
Carbotrap® 300 Glass-Fritted Thermal Desorption Tube, 1/4 in O.D. x 3.5 in L (30141-U)
desorption process
350 °C with 10 min hold
transfer line/valve temp.
180 °C
column
SPB®-HAP, 60 m x 0.32 mm I.D., 4 μm (25020-U)
oven
40 °C (3 min), 12 °C/min to 200 °C (20 min)
detector
MSD
MSD interface
210 °C
carrier gas
helium
dry purge
15 min
Descripción
Descripción general
Qualitative volatile headspace outgassing from purple nitrile gloves using the ATIS system with analysis by thermal desorption.
Información legal
Carbotrap is a registered trademark of Merck KGaA, Darmstadt, Germany
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany