GC Analysis of Pesticides in Wine on SLB®-5ms after SPME using 85 μm Polyacrylate Fiber
CONDITIONS
sample/matrix
white wine spiked with 50 ppb pesticides
SPME fiber
85 μm polyacrylate (57304)
extraction
immersion, room temp (30 min)
desorption process
250 °C for 5 min
column
SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
oven
60 °C (1 min), 15 °C/min to 100 °C, 7 °C/min to 300 °C (1 min)
MSD interface
325 °C
scan range
SIM
carrier gas
helium, 0.7 mL/min, constant
liner
0.75 mm I.D. SPME liner
Descripción
Información legal
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany