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GC Analysis of 5-Amino-1,3,3-Trimethylcyclohexanemethylamine Enantiomers (N-TFA Derivatives) on Astec® CHIRALDEX A-TA

GC Analysis of 5-Amino-1,3,3-Trimethylcyclohexanemethylamine Enantiomers (N-TFA Derivatives) on Astec® CHIRALDEX™ A-TA suitable for GC

Materiales

columna analítica

Referencia del producto
Descripción
Precios

Astec® CHIRALDEX A-TA Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.12 μm

patrón

Referencia del producto
Descripción
Precios

5-Amino-1,3,3-trimethylcyclohexanemethylamine, mixture of cis and trans

≥99%

CONDITIONS

column

Astec CHIRALDEX A-TA, 30 m x 0.25 mm I.D., 0.12 μm (73003AST)

oven

160 °C

inj. temp.

250 °C

detector

FID, 250 °C

carrier gas

helium, 30 psi

injection

1 μL, 80:1 split

sample

3 mg/mL racemate in methanol
peaks 1 & 2: first enantiomer pair
peaks 3 & 4: second enantiomer pair

Descripción

Información legal

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC