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Merck

21099-U

Supelco

GC Stationary Phase

phase SE-30, bottle of 10 g

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About This Item

Código UNSPSC:
23151817
NACRES:
SB.54

Agency

meets requirements for USP G2

envase

bottle of 10 g

Parámetros

temp. range at 50-300 °C

técnicas

gas chromatography (GC): suitable

grupo activo de la matriz

SE-30 phase

solubilidad

chloroform: soluble

tipo de columna

packed GC

Descripción general

GC methods are divided into two classes depending on the nature of stationary phases; gas-solid chromatography (GSC) and gas-liquid chromatography (GLC). GSC has solid adsorptive material and solute particles are removed from mobile phase by electrostatic forces. GLC has a thin layer of liquid coated or bonded on the surface of an inert particle or on the walls of the column where solute particles are retained in the liquid phase based on their partition coefficients. The primary necessity of a stationary phase is to provide sample separation sustaining phase integrity over a reasonable period of time. It should be stable for the chemical and thermal changes. Selectivity, peak symmetry, analysis time, degree of separation, peak tailing are a few parameters that should be considered before choosing a stationary phase. SE-30 is a dimethyl silicone elastomer. It is widely suitable as liquid phase got GLC.
Synthesized specifically to be purer, of narrow molecular weight range, and without trace catalysts or impurities for use as a GC stationary phase.

Aplicación

SE-30 was used as stationary phase for the analysis of the thiohydantoins using GC. It may also be used as liquid phase in identification of the single polychlorinated biphenyls (PCB) components by comparing their retention indices, using high-resolution thin-film glass capillary gas chromatography coupled with electron-capture detector.

Código de clase de almacenamiento

10 - Combustible liquids

Clase de riesgo para el agua (WGK)

WGK 3

Punto de inflamabilidad (°F)

Not applicable

Punto de inflamabilidad (°C)

Not applicable

Equipo de protección personal

Eyeshields, Gloves


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Analysis of polychlorinated biphenyls (PCB) by glass capillary gas chromatography.
Ballschmiter
Fresenius' Zeitschrift fur Analytische Chemie, 302, 20-31 (1980)
A C Moffat
Journal of chromatography, 113(1), 69-95 (1975-03-12)
The dimethyl silicone elastomer SE-30 has been chosen as the preferred liquid phase for the gas-liquid chromatographic analysis of drugs, and retention index data have been compiled for 480 drugs and commonly occurring chemicals such as plasticisers. The inter-laboratory variation
Analysis of amino acid phenylthiohydantoins by gas chromatography.
J J Pisano et al.
The Journal of biological chemistry, 244(20), 5597-5607 (1969-10-25)
James P. Lodge, Jr.
Methods of Air Sampling and Analysis, 98-98 (1988)
David B. Troy, Paul Beringer
Remington: The Science and Practice of Pharmacy, 605-605 (2006)

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